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GCMS analysis results for sample AD26625, Dec 10 2001

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Laboratory report documenting GCMS analysis of sample AD26625 identifying unknown compounds on December 10, 2001.

NYC-WTC_000031920–000031939

Folder label: “GCMS X 11/7/01 A 12/6/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

'Data File C:\HPCHEM\l\DATA\DEC0601\26625.D Vial: 8 Acq On 6 Dec 2001 4:34 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 2-Butanol, 3-methyl-, (S)- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

7.18 6.49 ng/uL 2096230 1,4-Dichlorobenzene-d4 11.88

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Butanol/ 3-methyl-, (S)- 88 C5H120 001517-66-4 42 2 2,3-Butanediol 90 C4H10O2 000513-85-9 33 3 N-Ethylformamide 73 C3H7NO 000627-45-2 9 4 2-Butan , 3-methyl- 88 C5H120 000598-75-4 9 Abundance Scan 255 (7.178 min): 26625.D (-) m/ z 45.10 100.00% 45

5000- 61 73 -----

6.80 7.00 7.20 7.40 7.60 " I''" I ............ A ... 88......................... n । pi 1111111 p 111 p 111 p 111 p । ■ । p ■ 11 p । ■ 11 207 m/ z 4 3.00 64.11% m/z-> 10 20 30 40 50 60 70 80 90 100110120130 140 150160170180190200210 Abundance #852: 2-Butanol, 3-methyl-, (S)- 45

.—s — , . S i . । , -Ti । । i 5000 - i 6.80 7.00 7.20 7.40 7.60 i m/z 73.05 36.22% i। 27 55 73 mpmp 11 ’| " I 1 87 I ‘ " I'"' I TTTTTT | Mt . p i H | . I ii | . • • • |

m/z-> 10 20 30 40 50 60 70 80 90 100110120 130 140150 1 60 1 70180 190 200 210 Abundance #917: 2,3-Butancolol i 45

6.80 7.00 7.20 7.40 7.60 5000 m/z 61.10 35.93% 29 19 57 T’TETTTTTITTTTTTTTTTTTTTT 75 90_____________________ __________ TTTT’TTT " " I' " ' I " ' 11 " '11" " I ’ " ' I' *'11 • i' 11 ' 1111" P11 r) 11111 m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200210 Abundance I 30 #292: N-Ethylformamide • । ■ • • • । • 6.80 7.00 -P— 7.20 7.40 7.60 73 m/z 44.05 13.65% 5000 44 58 i I I , m/z-> 5 | ■ i.. । .’i i. | ■ b . |. I r k ।।।।। 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 210 ।।। ।। 6.80 7.00 J 7.20 == 7.40 7.60

26625.D NP112701.M Fri Dec 07 14:48:45 2001 Page 8

NYC-WTC_000031934

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NYC-WTC_000031934Source: NYC Law Department, mirrored locally

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