GCMS Analysis Report for Sample AD26387, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26387.D vial: 13 Acq On : 30 Nov 2001 11:08 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise 2 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Cyclopentanol, 1-methyl- Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 6.14 1.49 ng/uL 719464 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual l Cyclopentanol, 1-methyl- 100 C6H120 001462-03-9 28 2 Cyclopentanol,/1-methyl- 100 C6H120 001462-03-9 9 3 Propanoic acid, 2-methyl-, anhydrid 158 C8H14O3 000097-72-3 9 4 2-Furanmethanamine, tetrahydro- 101 C5H11NO 004795-29-3 9 Abundance Scan 142 (6.140 min): 26387.D (-) m/z 71.05 100.00% 71

5000 43

V,1 ' ' 11 1 1 1 1 1 1' ' TII 11001.7 , 57 ! . ....... 81................. 100......... 5.80 6.00 6.20 6.40 ........................... 38, 1 ■ ■ ■ । ■' ■ ■ । • ■ ■ ■ । ■ ■ ■ ■ ।' ■ • ‘ । ■ ■ ■ ■ ।' ■" i rrrpTTTpTTTpTnTTTTTJTTTT^^ m/z 43.05 43.53% m/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63340: Cyclopentanol, 1-methyl-

5000 43

58 71

‘ 1 I ‘

m/z 5.80 A ‘ 1 1 1 1 ' I 1 1 1 1 I 1 1 1 1 1 1 6.00 41.05 6.20 6.40 24.21% 85 1’011111151319—01100101000111111 53 rk Hr TJTHmm -p-n-rj nh 100 m/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #1511: Cyclopentanol, 1-methyl- 71 ‘ ' i ‘ ‘ ■ i ' r ■ ' i 1 1 1 • i ‘ ■ i ‘ 43 5.80 6.00 6.20 6.40 5000 58 m/z 42.10 19.13%

85 15.. 2 53,|L h _ 100 .... ।.... [.,.. (..,. ।. 1., (. 1111..., ।. 1.,....!.. I., 1111 r 4! i j. l.. l. ■ t > ■ 11 [ 111111111H 11111 n i (> u 111111 m/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #11901: Propanoic acid, 2-methyl-, anhydride —rrr T | IT-I1 l 1161111881 | T 71 5.80 6.00 6.20 6.40 m/z 39.00 10.45% 43 5000

m/z—> 27 1 39. i . 55 i i i 11 » i i t ( i 11 11 m 11 j I I J r j r u I | i 11 IJ I I I I | i i i i p m t | u i r 11 11 i । : i J J 11 11 11:11» pr: 11 11 CT 11 1 11 |! 11 I j | | 11 |J I i 1 [ 5 10 15 20 25 3035404550556065 70 75 80859095 100105 WRAA 5.80 6.00 6.20 6.40

26387.D NP112701.M Tue Dec 04 10:39:13 2001 Page 4

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