GCMS Analysis Report for Sample AD26387, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26387.D vial: 13 Acq On : 30 NOV 2001 11:08 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 3-Hexanol Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 6.73 0.42 ng/uL 202981 1,4-Dichlorobenzene-d4 11.89 Hit# of Tentative ID MW MolForm CAS# Qual 1 3-Hexanol 102 C6H14O 000623-37-0 83 2 3-Hexanol 102 C6H140 000623-37-0 83 3 3-Heocanol 102 C6H140 000623-37-0 78 4 3-Hexanol 102 C6H140 000623-37-0 64 Abundance Scan 206 (6.727 min): 26387.D (-) m/z 59.10 100.00% 55 59

5000 73 43 ........ -A 39 69 6.40 6.60 6.80 7.00 -— — ’ —

' i ■ ■ “ i ‘ ■ i ■ “ ' i ■' m/z 55.10 77.94% ■ ■ i ■ miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #63531:3-Hexanol

55 59 5000 73 ' 71 P IT Tr p . . . 1 6.40 6.60 6.80 7.00 43 m/z 73.05 46.53%

miz-> 20 25 30 35 39 MHHt 40 45 50 —55H-8+ 60 65 70 75 80 85 90 ' I “ “ I " ■ ■ i " ' ■ i ■ ■

Abundance #63528:3-Hexanol 55 59 ............ _ —1 73 6.40 6.60 6.80 7.00’ ' ‘ ' 5000 m/z 43.00 31.03% 31

27

n/z-> 20 .... T 25 30 45 TIPTT TH + 84 ■'I > > > I I I I I > I 1 I t | । । 1 i | i n i । i TIIrT 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #63527:3-Hexanol "TTTTTTTTTum 50 6.40 6.60 6.80 7.00 55 m/z 41.10 23.37%

JUUVA 5000 73 31

27 45 TII" -H — ‘ £‘‘‘11" " 45 " aj ’ —4■ | • >111 • • • > 111 1111" I " 84 '1111 “ I'1 TTImmTTTT m/z—> 20 25 30 35 40 55 60 65 70 75 80 85 90 6.40 6.60 6.80 7.00

26387.D NP112701.M Tue Dec 04 10:39:14 2001 Page 5

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