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GCMS analysis results for sample AD26829, Dec 10 2001

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Laboratory report documenting GCMS analysis of sample AD26829 identifying unknown compounds on December 10, 2001.

NYC-WTC_000032202–000032222

Folder label: “GCMS X 11/7/01 A 12/6/01

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Scanned page image, NYC-WTC_000032216
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26829.D Vial: 6 Acq On 6 Dec 2001 2:44 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params.: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 3-Hexanol Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

6.71 0.52 ng/uL 148836 • 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanol 102 C6H140 000623-37-0 83 2 3-Hexanol 102 C6H140 000623-37-0 83 3 3-Hexanol 102 C6H140 000623-37-0 83 4 3-Hexanol 102 C6H140 000623-37-0 83 Abundance Scan 204 (6.710 min): 26829.D (-) m/z 59.1.0 100.00% 55 59

5000 73 43 ---A-- -AA 39 6.40 6.60 6.80 7.00

m/z-> + — T TTT TT 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 m/ z 55.10 89.66% Abundance #63529: 3-Hexanol 59 55

5000- 31 73 M II-Tm 27 6.40 6.60 6.80 7.00 m/ z 73.05 41.80% 44 102 m/z-> T’T TH 4 TT Tri T‘rrrTE"‘‘I‘‘1‘1‘11711 I TTT 11 T‘ 20 25 30 35 40 45 50 55 60 65 70 75 80 '85 90 95 100 105 110 Abundance #63528: 3-Hexanol 59 55 / TT 6.40 6.60 6.80 7.00 73 5000- m/z 43.05 31.36% 31

27 45 84 T I . . . . I . . . !p . . . ! . . . . I > . i I I . . . . I I . . I I I . I q I . > , | , I ( . . I . | y i'' " i" ■ ■ i'' " r " ■ i m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63527: 3-Hexanol ■ ■ i 1 ■ J V 55 59 — 6.40 6.60 6.80 7.00 m/ z 41.05 25.97%

VUNA 5000 73 31

27 45 84 -P i■■ ■ ■ i — ill TTT I 1T TTUTT i" 111 T‘ ‘m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 6.40 6.60 6.80 7.00

26829.D NP112701.M Fri Dec 07 14:54:37 2001 Page 8

NYC-WTC_000032216

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NYC-WTC_000032216Source: NYC Law Department, mirrored locally

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