GCMS calibration table for TCLP analysis, Dec 6 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\LBB.D Vial: 14 Acq On 6 Dec 2001 10:00 pm Operator: GALOS Sample lab blank 11/8 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 3-Hexanol Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

10.32 1.06 ng/uL 391770 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 , Tentative ID MW MolForm CAS# Qual

1 3-Hexanol 102 C6H140 000623-37-0 38 2 3-Hexanol 102 C6H140 000623-37-0 37 3 3-Hexanol 102 C6H140 000623-37-0 37 4 3-Hexanol 'Abundance/ 102 C6H140 _______ 000623-37-0 32 Scan 597 (10.318 min): BB.D (-) m/z 43.05 100.00% 43 59 5000 55 73 85

m/z-> TT 1 •" ' I " '11 4 H Hmm 39 100 TTTTTTTTTTT TT 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 IT 10.00 m/z 10.20 59.1.0 10.40 10.60 54.30% Abundance #1762: 3-Hexanol

i 55 59 31 5000 27 43 73 KP 10.00 10.20 10.40 10.60 m/ Z 44.65% " r " ■ r ■" i 11111111 i l I' ■' > I 1’ ’ I............. | I I I I | ! < I I ( I ) . • | I I I . | 102 I' •'' I TT 55'10 m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63529: 3-Hexanol 59 : 55 10.00 10.20 10.40 10.60 31 m/z 57.10 5000 73 35.43% 27

44 102 11 ‘ " I TI I.... I(. I.. 1.... 1.... I ■ TTTTTTTTTTTTTTTTTT I"11 i TT m/z->20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance i #63527:3-Hexanol —50 59 4. AAA 10.00 10.20 10.40 10.60 ! m/ z 32.50% 41.10 5000 73 31

27 ' r ' " r " ' I ‘ " i" + TTTTTT TDTTIUTTTTT m 45 84 ।■■ ■ ■ । ■ ■ ■ • । • ■ ■ •।। ■ TTCTEIK—rrT m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 10.00 10.20 10.40 10.60

LBB.D NP112701.M Wed Dec 12 08:19:15 2001 Page 9

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