GCMS calibration data for TCLP analysis dated December 7, 2001

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Data File C:\HPCHEM\1\DATA\DEC0 701\LB.D Vial: 2 Acq On 7 Dec 2001 7:01 pm Operator: GALOS Sample gc/ms unknown 11/6 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 3-Hexanol Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 6.68 0.77 ng/uL 237285 1,4-Dichlorobenzene-d4 11.88 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexan 102 C6H140 000623-37-0 83 2 3-Hex. /lol 102 C6H140 000623-37-0 83 3 3-He: nol 102 C6H140 000623-37-0 83 4 3-H anol 102 C6H140 000623-37-0 64 Abundance Scan 201 (6.683 mln): LB.D (-) m/ z 59.10 100.00% 55 59 —

5000 73 — -1 — ■ — 43 39 | 69 . 6.40 6.60 6.80 7.00 —P -PPP >j 1111111 11111 - TIH 11—9—— rn/z 55.10 81.46% miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #63527:3-Hexanol . oo 59

5000 73 T . v . । . r. . 1 1T । r . . r 31 6.40 6.60 6.80 7.00 m/z 73.05 40.91% 27 45 84 — — 11 — r — ' 1111111 ■ > ■ 111 11 ■ • • ■ i ■111 ■■ । ।11111'1 ■11" 111'1111 miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #63528: 3-Hexanol 59 55 • • • • | » • • • | • ■ TT' | । . 1 I • 6.40 6.60 6.80 7.00 73 5000 m/z 43.05 19.44% 31

27 AE 45 . 84 ’ ’ I ‘11 * J "‘‘‘I . . . I . . . rf-mt-p .. . I > ... I rtTT-fTTT-rp-> . . | ... I I ... . ]Trrrp-rrrp-r m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 80 Abundance #63531:3-Hexanol I I I I TT I I TTITTT TTInI

55 59 6.40 6.60 6.80 7.00 m/z 41.05 19.34% 15.34

m/z-> 5000

.।।।।. 11.1111... • । *' 20 25 30 35 39 40 43

45 50 —+ 55 ................... 60 65 70 73

I ■ ■ ■' i ■ ■ ■ ■ i ■1 11 ■ • •1 j • n . ।. ■.. ।■ 75 80 85 90 WO *n1“11+1*111218T IIE8 6.40 6.60 6.80 7.00

LB.D NP112701.M Thu Dec 13 11:28:36 2001 Page 8

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