GCMS calibration data for TCLP analysis dated December 7, 2001

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Instrument output file listing calibration standards and response factors for various compounds used in the December 7, 2001 analysis.

NYC-WTC_000031665–000031684

Folder label: “GCMS X 11/6/01 A 12/7/01”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C : \HPCHEM\ 1 \DATA\DEC0 7 01 \LB. D Vial: 2 Acq On 7 Dec 2001 7:01 pm Operator: GALOS Sample gc/ms unknown 11/6 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 2-Butanol, 3-methyl-, (S)- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.16 11.83 ng/uL 3667350 1,4-Dichlorobenzene-d4 11.88

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Butanol, 3-methyl-, (S) - 88 C5H120 001517-66-4 42 2 1,2- Propanediol , 3 -methoxy- 106 C4H10O3 000623-39-2 36 3 2,3-Butanediol 90 C4H10O2 000513-85-9 33 4 2-Butanol, 3-methyl- 88 C5H120 000598-75-4 9 Abundance Scan 253 (7.159 min): LB.D (-) m/z 45.10 100.00% 45

5000 61 73

6.80 7.00 7.20 7.40 7.60 5,1 14 1111 + 88 35 rryTTrrp-mrp- 207 ।।.... । ....p... ।.... ।.... |.... ] .11 m/z 43.00 67.70% miz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #852:2-ButanoI, 3-methyl-, (S} 45

.................. .................. — 5000 • I ' ' 1 • l ‘ 1 1 ‘ I ■ ' ■ • I ' 6.80 7.00 7.20 7.40 7.60 55 73 m/ z 61.10 35.20% 1

miz-> 27. _......... ,1..... 87 lH“l 1 ■ i ■1 “ i‘ “ 'i ““ i • • * • । ■pTTTpTTTp-rTTpTrTp-rrrprrrrrrrrrp-rrrjTTTTp-^^ 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #63660: 1,2-Propanediol, 3-methoxy- 45 • ' i • ■ ' ■ i ■ • • i • • • • l» 6.80 7.00 7.20 7.40 7.60 5000 75 m/z 73.0, 34.30% 31 61 15 TIUg i""i 4 ।.... f.... j. i11.. t...8811.... ।. i.. 1.... ।..., j.... ।. 11 > 11... ।.... ।.... ।.... 11. ।. ।.... . I

m/z-> 10 2030405060 70 8090 100110120130140150160170180190200210 Abundance #917:2,3-Butanediol । i • • • • । • 1 1 I 1 1 1 1 1 r 45 6.80 7.00 7.20 7.40 7.60 m/z 44.0.5 14.23% 5000-

29 | I .. 19 1 457 75 90 "i > ■1 • । ■ ■" । ■ IEITETET’T ■. । । t f i . fi TT i j r.'. । f. । . . । । miz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 6.80 7.00 7.20 7.40 7.60

LB.D NP112701.M Thu Dec 13 11:28:38 2001 Page 9

NYC-WTC_000031679

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