GCMS analysis sample AD26537, non-target compounds, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\l\DATA\DEC0701\26537.D Vial: 4 Acq On 7 Dec 2001 8:51 pm Operator: GALOS Sample gc/ms unknown 11/6 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 3-Hexanol Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 6.67 0.90 ng/uL 240899 1,4-Dichlorobenzene-d4 11.88

Hit# of 5 'entative ID MW MolForm CAS# Qual

1 3-Hexanol 102 C6H140 000623-37-0 83 2 3-Hexanol 102 C6H140 000623-37-0 74 3 3- xanol 102 C6H140 000623-37-0 74 4 3-Hexanol 102 C6H140 000623-37-0 74 Abundance..... Scan 199 (6.668 min): 26537.D (-) m/ z 59.10 100.00% 55 59

5000 73 41 1 ‘ 1 ‘ ’ I 6.40 6.60 6.80 7.00 ------- — Hr TT —mmmmTTT m/z !55.05 77.46% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63531: 3-Hexanol ............ T 55 59 5000 73 —PArwAl ov e 6.40l 6.60 6.80 7.00 43 m/z 73.05 41.79% 39 1 69 l 111 iTTp-m TU TPm Hu rp-rrn *]] miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63528; 3-Hexanol 59 55 - T PPPI PPP 6.40 6.60 6.80 7.00 73 5000 m/z 41.10 20.52% 31

m/z-> Abundance _4 27 ; 45 ■ 84 ,. ।. 11..., 1।....,;.. 1 j.... 111111 > i 111 > 11■1111111llI)in 111 n11n111■i■1111111111■11111!i 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 #1762:3-Hexanol 55 59 \MN 1640 6.60 6.80 7.00 m/z 56.10 8.26% 31 5000 27 43 73

m — m H — +44 H m — mm -192- AMheAA miz—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 6.40 6.60 6.80 7.00

26537.D NP112701.M Thu Dec 13 11:27:23 2001 Page 8

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