GCMS comments for sample AD26476 showing no non-target compounds

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0701\26476.D vial: 6 Acq On 7 Dec 2001 10:40 pm Operator: GALOS Sample gc/ms unknown 11/6 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title 208 625/TCLP calibration table Library C: \DATABASE\NBS75K. L ********************************************************************* Peak Number 8 3-Hexanol Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

6.68 1.04 ng/uL 372957 1,4-Dichlorobenzene-d4 11.87

Hit# Of 5 'entative ID MW MolForm CAS# Qual

1 3-Hexanol 102 C6H140 000623-37-0 83 2 3-Hexanol 102 C6H140 000623-37-0 74 3 3-Hexanol 102 C6H140 000623-37-0 74 4 3-Hexanol 102 C6H140 000623-37-0 64 Abundance Scan 201 (6.683 min): 26476.D (-) m/ z 59.05 100.00% 55 59

5000 73 43 ■ ■ ■ ■ ■ । ■ i' ' ■ ■ i1' ■ 1 r । 1 ■ ' ■

39 6.40 6.60 6.80 7.00

m/z-> 20 25 30 35 --HHH 40 51 TTTr + 69 1 84 |, TITITT 1 i ■ ■ ■ ■ i' 1 1 111 1 1 1 1 1 1 45 50 55 60 65 70 75 80 85 90 m/ z 55.10 77.02% Abundance #63531: 3-Hexanol 59 55

5000- 73 -A— A , —====+ — 6.40 6.60 6.80 7.00 43 m/z 73.05 43.60%

m/z-> 20 25 30 35 39 HHit....... —+ ,............ 69 , 1111111111 40 45 50 55 60 65 70 > । > • ■ • । ■ • • ■ । ■ • ■ ■ । ■ 75 80 85 90 Abundance #63528: 3-Hexanol 59 55 i 6.40 6.60 6.80 7.00 73 5000 m/ z 43.05 27.91% 31

27 45 I 84 l,.i . 11'1111 ‘1 ■ ■ । ■ ■ ■ ■ ।''' ■ । ■ ■ ■' ।1 ■'11' 1 l ' ' '' i ' '' ' I'' ' ' i' 11 • ■ ■' i • ■ ■11'11' 11 m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #63527: 3-Hexanol > • i > ■ 6.40 6.60 6.80 7.00 55 5 m/ z 41.10 21.13% 5000 73 31

m/z-> 27 —4 • i • ■ > • । ■ I ■ ■ 11 • ■ ■ i ■ tt — 20 25 30 35 40 45 50 55 60 65 70 84 45 • i ■ > ■ • | • ■ ■ • i •

75 80 85 90 1 i ' ■ ■ ■ i 1 1 ■ ' i 1 1 1' i ' W 6.40 6.60 6.80 7.00

26476.D NP112701.M Thu Dec 13 11:20:53 2001 Page 8

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