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GCMS comments for sample AD26476 showing no non-target compounds

Machine-extracted title · confidence 100%

Analysis report dated December 16, 2001, stating that mass spectrometry of sample AD26476 revealed no non-target compounds.

NYC-WTC_000031707–000031728

Folder label: “GCMS X 11/6/01 A 12/7/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC0 7 01\26476.D Vial: 6 Acq On 7 Dec 2001 10:40 pm Operator: GALOS Sample gc/ms unknown 11/6 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 2-Hexanone Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

6.55 0.78 ng/uL 280122 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanone/ 100 C6H120 000591-78-6 90 2 Oxirane,/2-methyl-2-(1-methylethyl) 100 C6H12O 072221-03-5 64 3 2-Hexanone 100 C6H120 000591-78-6 64 4 2-Hexanone 100 C6H120 000591-78-6 64 Abundance Scan 187 (6.554 min): 26476.D (-) m/z 43.00 100.00% 43

5000

r "M +384 + 51+ 72 58

i" " i 85 100 TTTTTTT M 6.20 m/z 6.40 58.10 6.60 6.80 52.47% 7.00

m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1556:2-Hexanone 43

58 5000 • ' l 1 • ■ ' I 1 11 1 j ' I I • I I ' 6.20 6.40 6.60 6.80 7.00 m/z 41.10 14.99% 27 39 71 85 100 T‘‘T > ।. 111J.. 111 —r TT T m 111' ’ r — r 1" i m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1530: Oxirane, 2-methyl-2-(1-methylethyl)- 43 58 J 6.20 6.40 6.60 6.80 7.00 5000- m/ z 57.10 10.53% 71

30 52 J|. 66 | 85 100 I r " ' i"'' i ■''' I 1' " 11 ■ • • ■ । • • ■ ■ । ■ i ■ • •' r " ' r " ■ i TT 111 • ’ " I " " I m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63385:2-Hexanone 43 6.20 6.40 6.60 6.80 7.00 m/z 100 05 7.83% 5000 58

m/z-> 29 39 TPT ml r ... '' I''111111 71 85 111111।11 100 ।|।। 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 4 6.20 6.40 W 6.60 6.80 7.00

26476.D NP112701.M Thu Dec 13 11:20:49 2001 Page 7

NYC-WTC_000031721

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NYC-WTC_000031721Source: NYC Law Department, mirrored locally

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