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GCMS comments for sample AD26475 showing no non-target compounds

Machine-extracted title · confidence 100%

Analysis report dated December 16, 2001, stating that mass spectrometry of sample AD26475 revealed no non-target compounds.

NYC-WTC_000031685–000031706

Folder label: “GCMS X 11/6/01 A 12/7/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC0 7 01\26475.D Vial: 5 Acq On 7 Dec 2001 9:45 pm Operator: GALOS Sample gc/ms unknown 11/6 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 7 2-Hexanone Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

6.55 0.70 ng/uL 197213 1,4-Dichlorobenzene-d4 11.88

Hit# Of 5 ntative ID MW MolForm CAS# Qual

1 2-Hexanone 100 C6H120 000591-78-6 64 2 2-Hexanone 100 C6H120 000591-78-6 53 3 2-Hexanone 100 C6H120 000591-78-6 53 4 Oxirane, 2-methyl-2-(1-methylethyl) 100 C6H120 072221-03-5 50 Abundance Scan 187 (6.554 min): 26475.D (-) m/z 43.00 100.00% 43 58 5000

391 85 100 6.20 6.40 6.60 6.80 7.00 53 | 71 TH+ tp-rr TWmmmTT l1 > • • । ■ ■ ■ ■ | • ■ ■ ■ । ■ ■ ■ ■ । m/z 58.10 60.53% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63384: 2-Hexanone 43

5000 - 58 — — 1 1 I I TP_1 I I I I TIM II __ 6.20 6.4 6.60 6.80 7.00 29 m/z 41.10 12.49% 39 ; 71 85 100 *II—nuIp—ur — ....... TI **PPTT PI+T i" ■ ■ i " " I" " r " ' i m/z—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1556; 2-Hexanone 43 MMA. 6.20 6.40 6.60 6.80 7.00 58 5000 m/z 57.10 10.46%

27 71 85 100 39 .1 TTTTTTTTTTgu I ’1" 1” r il i" ■11 " i " " I" ' ‘ i m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63385:2-Hexanone 43 6.20 6.40 6.60 6.80 7.00 m/z 85.0,5 7.24% 5000 - 58

29 39 71 85 100 - — 1PPpmpe 1T TPP TVOIUOOTITTTTTTTTT m/z--> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.20 6.40 6.60 6.80 7.00

26475.D NP112701.M Thu Dec 13 11:19:36 2001 Page 7

NYC-WTC_000031699

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