GCMS analysis results for sample AD26682, Dec 10 2001

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Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC0 5 01\26682.D Vial: 2 Acq On 5 Dec 2001 9:41 am Operator: GALOS Sample gc/ms unknown 11/7 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 3-Hexanol Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

6.67 0.47 ng/uL 161913 1,4-Dichlorobenzene-d4 11.86

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 3 -Hexanol 102 C6H140 000623-37-0 83 2 3 -Hexanol 102 C6H140 000623-37-0 74 3 3-Hexanol 102 C6H140 000623-37-0 64 4 3 -Hexanol 102 C6H140 000623-37-0 64 Abundance Scan 199 (6.669 min): 26682.D (-) m/ z 59.10 100.00% 55 59

5000 73 41 —iPAT 1 44 6.40 6.60 6.80 7.00

m/z-> T-i-|->-n-s-p-rT-t-r-r-n->-p- 20 25 30 35 —H H — ' I'1 ■ |।।. 1111 40 45 50 55 60 65 70 75 80 85 90 । । ।< m/z 55.10 79.42% Abundance #63531: 3-Hexanol 59 55

5000- 73 ?- P 6.40 6.60 6.80 7.00 43 m/z 73.05 44.09% ................................... 39 1 i 1111 ।1 —---%%++ TI’EETTTTIT’rrI1—T m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #63528: 3-Hexanol 59 55 6.40 6.60 6.80 7.00 73 5000- m/z 41.05 24.09%

JUU 31

27 45 84 . । , , . , | i-, ri | r, | m rp 11—nu—uO’Twrrtrrn——n’ptpprrrprnuterr m/z-> 20 25 30 35 40 45 50 55 60__ 65 70 75 80 85 90 Abundance #63527: 3-Hexanol 50 59 — | 6.40 6.60 6.80 7.00 m/z 43.05 19.76% 5000 - 73 31

111 - 27 45 TPPPT T 4m ■ 111 > 1111111 > I 84 11 ' ' ' ■ i ■ • ' 11 1 ' '' i ' ' AA==...... 4 miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 6.40 6.60 6.80 7.00

26682 .D NP112701.M Fri Dec 07 13:13:24 2001 Page 7

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