GCMS analysis results for sample AD26682, Dec 10 2001

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Library Search Compound Report

Data File . C:\HPCHEM\1\DATA\DEC0501\26682.D Vial: 2 Acq On 5 Dec 2001 9:41 am Operator: GALOS Sample gc/ms unknown 11/7 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 2-Hexanone Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

6.54 0.59 ng/uL 204138 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanone 100 C6H120 000591-78-6 91 2 2-Hexanone 100 C6H120 000591-78-6 91 3 2-Hexanone 100 C6H120 000591-78-6 90 4 2-Hexanone 100 C6H120 000591-78-6 90 Abundance Scan 185 (6.541 min): 26682.0 (-) m/z 43.0,0 100.00% 43

5000 58

391 85 100 6.20 6.40 6.60 6.80

m/z-> mH +51 — 71 — 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 I ■ ■ ■' r ''' I" " r'" i m/z 58.10 47.92% Abundance #63384:2-Hexanone 4)3

- 1 — -

5000- 58 6.20 6.40 6.60 6.80 29 m/z 41.05 14.62% 39 71 85 100 TTTTTTTTT TPTTTT TTTTr 11" " r ■ •' i'" ■ i " • ■ i " " I TTTTTTTTTTTTTTTTTTT m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance 43 #63385:2-Hexanone A 6.20 6.40 6.60 6.80 5000- 58 m/ z 57.10 12.65% 29 39 71 85 100 1 I... h f.... I... d I 11" 11" ■ ■ I ■ " 1 r ■ ■ ■ i TIT 11... । .... | , .. i ,। |।। m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63386: 2-Hexanone 5T 43 6.20 6.40 6.60 6.80 m/z 39.00 7.36% 5000 58

im/z-> ■ > i ■ ■ > >।• . 29

..... H 71 85 TTTTHTTTTTTT T’TTTTT I' " ' r ■ " i'' 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 100 i" " i —AA 6.20 AAA 6.46 6.60 6.80

26682.D NP112701.M Fri Dec 07 13:13:22 2001 Page 6

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