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GCMS Analysis Report for Sample AD26388, Dec 2001

Machine-extracted title · confidence 100%

Report documenting GCMS analysis of sample AD26388 with a note regarding unknown compounds.

NYC-WTC_000031452–000031472

Folder label: “GCMS X 11/5/01 A 12/1/01

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Scanned page image, NYC-WTC_000031463
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\NOV3 001\26388.D vial: 14 Acq On 1 Dec 2001 12:02 am Operator: GALOS Sample gc/ms unknown 11/3 Inst .: GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 3-Hexanone Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 6.47 0.58 ng/uL 256746 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Hexanone 100 C6H120 000589-38-8 87 2 3-Hexanone 100 C6H120 000589-38-8 86 3 3-Hexanone 100 C6H120 000589-38-8 78 4 3-Hexanone 100 C6H120 000589-38-8 56 Abundance Scan 177 (6.469 min): 26388.D (-) m/z 43.05 100.00% 43 57 71. 5000 100 • ■ • ■ । ■ ■ ■ • । •1 ■ ■ । • ■ ■ ■ । ■

85 6.20 6,40 6.60 6.80 .......................... .. hppoput Ipp Tung m/z 57.00 93.41% miz-> f. nt 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63358:3-Hexanone 43 57

71 5000 ‘ • i ‘ ■ i ‘ • i 1 ' ' ' i ' ■ ' ■ 6.20 6.40 6,60 6.80 100 m/z 71.05 54.57%

miz-> mmmmmm + Ip H TT-rrp-rrrp 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Hmm Abundance #1528: 3-Hexanone 43 57 ' 6.20 6.40 6.60 6.80 29 71 m/z 100.05 30.82% 5000 100

AAW , । ,85 ।11111111111 j 111111111111111 n । ] 11111111 > 111111 f11111111111111111111 >111>111111111 i 11111 mz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63356:3-Hexanone 29 43 57 6.20 6.40 6.60 6.80 m/z 41.05 25.79% 5000 71

100

“' i““i‘ —3, pT 1........ • ■ • ■ । ■ ■ ■' |1 ■.11'' ■' |' 111111' > i ■ 4 A , —, y y m/z—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.20 6.40 6.60 6.80

26388.D NP112701.M Tue Dec 04 10:40:23 2001 Page 6

NYC-WTC_000031463

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NYC-WTC_000031463Source: NYC Law Department, mirrored locally

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