GCMS analysis results for sample AD27189, Dec 2001

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Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DECO 7 01\27189.D Vial: 29 Acq On 8 Dec 2001 7:38 pm Operator: GALOS Sample gc/ms unknown 11/13 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Hexanone Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

6.59 0.49 ng/uL 130405 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 ntative ID MW MolForm CAS# Qual

1 2 - Hexane ie 100 C6H120 000591-78-6 90 2 2-Hexanone 100 C6H120 000591-78-6 90 3 2-Hexanone 100 C6H120 000591-78-6 80 4 2-Hexanone, 4-hydroxy-3-propyl- 158 C9H1802 062338-17-4 78 Abundance Scan 190 (6.585 min): 27189.D (-) m/ z 43.00 100.00% 43

5000-

341 i ’ •" r ‘" i A — TT 85 58

71 TTTTTfT- 100 AM 6.20 m/z 6.40 58.10 6.60 IIPTY 6.80 7.00 51.62% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63384:2-Hexanone 43

5000 58 6.20 6.40 6.60 6.80 7.00 29 m/z 41.05 16.24% 39 100

m/z—> i1" 11 tr i11'11 ‘1 *' r 71 TTTTTTTT 85 TTTTTTTr 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 m Abundance

5000- 43 #1556:2-Hexanone

58 MA , W . . 1

m/z 6.20 6.40 57.05 6.60 6.80 11.16% 7.00

_ 27 39 71 85 100 jTrrrp-rTTpT-TTprTTTpTnnrpn-rTpTnnYinnnTTTTTpnnnYr^^ 1 - । ।.. ii । r,.. । I rrp-T i• •*• i m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63385:2-Hexanone 43 6.20 6.40 6.60 6.80 7.00 m/z 100 .05 9.71% 5000 58

29

m/z-> mH 7 r 4+ iT 20 25 30 39

35 40 45 50 + 55 60 71 85 100 I'"' r " • r ■ " i ■ •" r " ' i1" ' r ' " i" " i 65 7C 75 80 85 90 95 100 105 6.20 6.40 6.60 6.80 7.00

27189.D NP112701.M Tue Dec 11 15:13:20 2001 Page 1

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