GCMS analysis results for sample AD26682, Dec 10 2001

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Library Search Compound Report

Data File C : \HPCHEM\ 1 \DATA\DECO5 0126682.D Vial: 2 Acq On 5 Dec 2001 9:41 am Operator: GALOS Sample gc/ms unknown 11/7 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 3-Hexanone Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

6.43 0.54 ng/uL 187117 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanone 100 C6H120 000589-38-8 90 2 3-Hexanone 100 C6H120 000589-38-8 86 3 3-Hexanone 100 C6H120 000589-38-8 86 4 3-Hexanone 100 C6H120 ________000589-38-8 64 Abundance Scan 173 (6.431 min): 26682.D (-) m/z 43.05 /100.00% 43 57

71 5000 - 100 39 6.00 6.20 6.40 6.60 6.80 " I'’"l" "T A 1 11" T TH 53. 85 ‘ ITTTTT +.... .. i""T m/z 57.1.0 90.43% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1528: 3-Hexanone 43 57

29 71 5000 6.00 6.20 6.40 6.60 6.80

1 100 rn/ z 71.05 51.18% 85 i1 • " i TH 11''' I T Th i11111

u m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63358: 3-Hexanone 43 57 6.00 6.20 6.40 6.60 6.80 71 m/z 100.05 24.16% 5000 - 100

85 I ' ' । | 1 1 ‘ | ’ • i >!■••• | i i f i | i t I . | I I I । | i . t r | । i I i pl . . | I i . » | . i i | ( i | < ' i " " i111' i TEET 'I miz-> ’Abundance 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 #63357:3-Hexanone A I ' • • ' I ’ 43 6.00 6.20 6.40 6.60 6.80 57 m/z 29 41.00 22.79% 5000- 71

mz-> mp 20 25 m 30 ....... I" " 11 1' i ‘' i " " I 35 40 45 50 55 60 65 70 ........... ?5........ 75 80 85 90 100

95 100 105 6.00 \M 6.20 6.40 6.60 6.80

26682.D NP112701.M Fri Dec 07 13:13:20 2001 Page 5

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