GCMS analysis results for sample AD26682, Dec 10 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0501\26682.D Vial: 2 Acq On 5 Dec 2001 9:41 am Operator: GALOS Sample gc/ms unknown 11/7 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 4 Tetrahydrofurfuryl chloride Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

6.08 0.72 ng/uL 249468 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tetrahydrofur ryl chloride 120 C5H9C1O 003003-84-7 50 2 Propanoic a d, 2-methyl-, anhydrid 158 C8H14O3 000097-72-3 40 3 2 -Furanme anamine, tetrahydro- 101 C5H11NO 004795-29-3 38 4 Cyclopentanol , 1-methyl- 100 C6H120 001462-03-9 25 Abundance Scan 135 (6.082 min): 26682.0 (-) m/z 71.05 100.00% 71

5000 43

-3 —L4 5.80 6.00 6.20 6.40 100 । ‘‘1, • , —I l t m/z 43.05 41.47% miz-> 20 • 80 30 90 100 40 50 60 70 110 120 Abundance #3704: Tetrahydrofurfuryl chloride 71

V 43 5000 5.80 6.00 6.20 6.40 27 m/ z 41.00 27.94% 49 55 62 ...... 1......... i-| i-r-r-rT "-r-rry■- ' i T’r ' i 1 1 77 120 m/z-> 20 30 40 50 60

A. AM 70 80 90 100 110 120 Abundance "11901: Propanoic acid. 2-methyl-, anhydride i 71 r-r-T-, T Trr-TT i T . p-m-p-rr < 5.80 6.00 6.20 6.40 43 I 5000 m/z 42.10 19.84% i i 27 ————55 38 . ■ । ' 1 ' । ■ ■ 'I ' ■ ——————— T । । । , , I , । । ...... > . । , m/z-> 20 30 40 50 60 70 80 90 100 110 120 A AA a/ w / Abundance I #1633: 2-Furanmethanamine, tetrahydro- - AA---- 71 5.80 6.00 6.20 6.40 m/z 39.00 11.62% 43 5000 30

m/z--> torrE 20 -..... — — 30 I

40 50 60 70। 58 4 H— 80 84

90 101 100 110 120 Lw A IAM 5.80 6.00 6.20) 6.40

26682.D NP112701.M Fri Dec 07 13:13:18 2001 Page 4

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