GCMS analysis result with unknowns, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26391.D vial: 7 Acq On : 30 Nov 2001 5:41 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Tetrahydrofurfuryl chloride Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 6.13 1.53 ng/uL 717632 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Tetrahydrofurfuryl chloride 120 C5H9C10 003003-84-7 39 2 2-Hepten-3-ol, 4,5-dimethyl- 142 C9H180 055956-37-1 38 3 Propanoic id, 2-methyl-, anhydrid 158 C8H14O3 000097-72-3 33 4 Cyclopent. ol, 1-methyl- 100 C6H120 001462-03-9 28 Abundance 7 Scan 141 (6.132 min): 26391 .D (-) m/z 71.05 100.00% 71

5000 43

5.80 6.00 6.20 6.40 —P + I I I 51444 T ■ I 70I1 1 ‘ 8081• . si 57 m/z 43.05 41.56% ■ 'i1 1 ' ‘ • ■ ‘ ‘ I ' i ‘ • 'I•'' i ‘ ‘ i ' ' m/z—> 10 20 30 40 50 60 90 100 110 120 130 Abundance #3704: Tetrahydrofurfuryl chloride 71

k 43 5000 1 . 1 1 1 . 1 1 1 1 1 1 1 1 ‘ ' p 1 ' 1 I 5.80 6.00 6.20 6.40 27 m/z 41.05 25.29%

miz-> ' 10 120 30 40 45.62. , 1 77...... 50 60 70 80 90 100 110 120 120 130 Abundance #8051: 2-Hepten-3-ol, 4,5-dimethyl- 71 . lj l. • ■ p • • < I > ‘ < l. " • I 5.80 6.00 6.20 6.40 5000 43 m/z 42.05 19.81% 27 15 55 81 I|, 100 109 124 miz—> Abundance Tt-"/E11-EEIC1CCI1-CCIEE"TSTT 10 20 30 40 50 60 T* —————— ■I '11•I•1''I' 80 90 100 110 120 130 #11901: Propanoic acid, 2-methyl-, anhydride 71 5.80 6.00 6.20 6.40 m/z 39.10 10.88% 43 5000-

m/z—> - 10 20 27 r 374 30 40 . i > ।, ।.. 11 ।, 11 j It- n mIr 50 55 60 70 80 90 11 • • .. 11 • • ■ I • ■ • • । • 100 110 120 130 Vo.ol 5.80 6.00 6.20 AA 6.40

26391.D NP112701.M Tue Dec 04 10:42:26 2001 Page 4

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