GCMS calibration table for TCLP analysis, Dec 6 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC06 01\LBB.D Vial: 14 Acq On 6 Dec 2001 10:00 pm Operator: GALOS Sample lab blank 11/8 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title 208 625/TCLP calibration table Library C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Tetrahydrofurfuryl chloride Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

6.14 0.99 ng/uL 366317 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 Tentative” ID MW MolForm CAS# Qual

1 Tetrahydrofurfu chloride 120 C5H9C1O 003003-84-7 50 2 2-Hepten-3-ol 4,5-dimethyl- 142 C9H180 055956-37-1 39 3 Cyclopentan , 1-methyl- 100 C6H120 001462-03-9 36 4 Propanoic acid, 2-methyl-, anhydrid 158 C8H14O3 000097-72-3 33 Abundance . Scan 141 (6.136 min): LBB.D (-) m/z 71-On5 100.00% 7|1

5000- 43

- - 44= 'm/z-> 10 20 30 4—5ul 40 50 60 80 701 90 |........................ 100................................. 100 110 120 130 5.80 m/z 6.00 43.05 6.20 6.40_____ 47.03%

N Abundance #3704: Tetrahydrofurfuryl chloride 71

k 43 5000- 11 5.80 6.00 6.20 6.40 27 m/Z 41.05 27.39% 49 55 62 77 120 ■ ' I T’r 1 1 1 ' ■ ■ 1 T’r , । । । . m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #8051: 2-Hepten-3-ol. 4,5-dimethyl- 71 V... SAL — MPPTTo 5.80 6.00 6.20 6.40 5000 - 43 m/z 42.10 19.90% 27 15 55 81 100 109 124 1 1 ' I ' miz-> 10 20 30__ 40 50 __ 60 70 80 90 100 110 120 130 'Abundance #1511: Cyclopentanol, 1-methyl- 71 5.80 —. -4A 6.00 6.20 6.40 43 m/ Z 39.00 12.41% 5000 - 58

m/z-> 15....... 1 27 , 1 i ' ' ' ‘ i ' ' ' ' i ' 10 20 30 ■ i • ■ ■ ■ i ' ' ' 40 50 LJ ' 60 I ■ ■ ' ' 1 1 70 85 - J......... 100.......................... 80 90 100 110 120 130 W......... AAA 5.80 6.00 6.20 6.40

LBB.D NP112701.M Wed Dec 12 08:19:06 2001 Page 4

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