GCMS calibration table for TCLP analysis, Dec 6 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\LBB.D Vial: 14 Acq On 6 Dec 2001 10:00 pm Operator: GALOS Sample lab blank 11/8 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title 208 625/TCLP calibration table Library C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Oxepane, 2,2,3-trimethyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

5.21 1.54 ng/uL 572320 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Oxepane, 2 ,2, 3 - trimethyl - 100 C6H120 023120-43-6 35 2 Pentane, 2, 3-dimethyl- 100 C7H16 000565-59-3 35 3 Pentane, 2,3-dimethyl- 100 C7H16 000565-59-3 35 4 Pentane, 2,3-dimethyl- 100 C7H16 000565-59-3 25 Abundance C Scan 40 (5.210 min): LBB.D (-) m/ z 41,05 100.00% 41 56

5000

45 71 =A---. 50 67 5.00 5.20 5.40 5.60

m/z-> 20 ?6+4 HTT 51+ + TTHT 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 ......... 100 m/z 43105 72.57% Abundance #1518: Oxepane, 2,2,3-trimethyl- 1 59 42 55 5000- T i nyPr 70 5.00 5.20 5.40 5.60 27 m/ z 56 10 70.47%

m/z-> '■r 4 TTT TT’TTTTT + .... . 85 100 IU—ut—"rrugtrmT 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63432: Pentane, 2.3-dimethyl- 56 43 —r 5.00 5.20 5.40 5.60 5000 71 m/z 59 ,10 68.79% 27 85 100 1 ■ i1 i • * >»t *»■ > I • • • -1 • • • * I • > • < i ■ •»• i l' "' I —IVBnummnmmoirronurmn m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63430: Pentane, 2,3-dimethyl- 43 56 5.00 5.20 5.40 5.60 m/ z 42 10 60.20% 5000 71 27 1i |' ■ i ■ ■ • ■ i ■ 85 -TT’IUUTTTTTTTTTTTrrTII 100 ‘‘1 n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 5.00 5.20 5.40 5.60

LBB.D NP112701.M Wed Dec 12 08:19:04 2001 Page 3

NYC-WTC_000032277