GCMS calibration table for TCLP analysis, Dec 6 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\LBB.D Vial: 14 Acq On 6 Dec 2001 10:00 pm Operator: GALOS Sample lab blank 11/8 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1-Butanol Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

5.16 0.89 ng/uL 330059 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Butanol 74 C4H10O 000071-36-3 32 2 1-Pentanol, 4-methyl- 102 C6H140 000626-89-1 25 3 Oxirane, (1-methylethyl)- 86 C5H10O 001438-14-8 17 4 Oxirane, ethyl-_____________ _______ 72 C4H80 000106-88-7 9 Abundance 7 Scan 34 (5.155 min): LBB.D (-) m/z 41. 05 100.00% 1 I 5000

71 II ' ‘ 1 TPI 45 5.00 5.20 5.40 5.60 : , m/z-> Ppwuunmu’tpoti 20 25 30 35 3E 150.531 + 60 6567 40 45 70 75 50 55 TPTTTtTttrITrtrII 80 85 90 95 m/z 56 . 10 83.21% Abundance #62584: 1-Butanol 41 56

5000 PII —r-r-T—r i r TT——mer 5.00 5.20 5.40 5.60 m/z 59.10 75.79% Pmm 38 । 4553_ m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63578; 1 -Pentanol, 4-methyl- 56 41 /........................... 5.00 5.20 5.40 5.60 69 5000- m/ z 42 . 05 67.29%

45 59 84 ' i ■' •' i''' ■ i''1' i ■'' ■ i1'' ■ i'TIIT ' ’ I ‘ ' I ■' TTPPIIPPTPWTTTT m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #721: Oxirane, (1-methylethyl)- ■ I ■ ' 1 । । । ■ I 41 56 5.00 5.20 5.40 5.60 m/z 43 . 05 66.38% 5000

miz--> 27 1 37 ■' । ■ ■ ■ ■ । ■1 ■ ■ । ■ • ■ ■ । ■ ■ ■ ■ ।

20 25 30 35 40 H... 505053155 A 45 60 70 75 85 90 95 65 80 5.00 N 5.20 7 i 7’ i ’i TI । , 5.40 5.60

LBB. D NP112701.M Wed Dec 12 08:19:02 2001 Page 2

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