GCMS calibration table for TCLP analysis, Dec 6 2001

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Data File C:\HPCHEM\l\DATA\DEC0601\LBB.D Vial: 14 Acq On 6 Dec 2001 10:00 pm Operator: GALOS Sample lab blank 11/8 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclohexane, methyl- Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

5.05 0.48 ng/uL 177088 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 entative ID MW MolForm CAS# Qual

1 Cyclohexane , methyl- 98 C7H14 000108-87-2 97 2 Cyclohexene, methyl- 98 C7H14 000108-87-2 97 3 Cyclohexane, methyl- 98 C7H14 000108-87-2 97 4 Cyclohexane, methyl - 98 C7H14 000108-87-2 53 Abundance Scan 22 (5.045 min): LBB.D (-) m/z 83.05 100.00% 55 83

41 98 5000- / 69 TT I'' 11'' ■ I • ' ' ' I ■' ■ • I

m/z-> 20 25 30 36 . TTTTT 35 40 ++ 45 +t mH + 50 55 60 65 70 75 80 85 • I" " I •' 90 trrrorr 95 100 105 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m/z ,55.10 97.77% Abundance #63236: Cyclohexane, methyl- 515 83

5000 98 —4 P ' '' I 1 T’TITT 42 4.90 5.00 5.10 5.20 5.30 5.40 5.50 27 70 m/ Z 41.0 661 TTTTT । ■ ■ ■ ■ । 'I' T’TT trer m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 'Abundance #1326: Cyclohexane, methyl- 55 83 r ■ ■ ■ i ■ ■ Tm-p-r 4.90 5.00 5.10 5.20 5.30 5.40 5.50 5000 98 m/z 98.05 48.25% 42 27 69

T‘I‘UIII-EITTTTITTTTTTTETTTTTTrT ‘trrTttr‘I‘“‘IN‘‘11111111ETTtO1111111"1116II06IE31—II31"T m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63235: Cyclohexane, methyl- TIEEICEEEtEECErTErErT 55 83 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m/ Z 42.0 39.51% 5000 98 42 69 27 I ml '11 'I"111'I TTmrpor " i " ■' i ■1" r ■" r " ■ i' " I'' " i' " n-p- Ipmpmpo TTTTTTTET TTTTT....... miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 4.90 5.00 5.10 5.20 5.30 5.40 5.50

LBB.D NP112701.M Wed Dec 12 08:19:00 2001 Page 1

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