GCMS results log, sample AD26985, Dec 11 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26986.D Vial: 32 Acq On 7 Dec 2001 3:19 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclohexane, methyl- Concentration Rank 15

R.T. EstConc Area Relative to ISTD R.T.

5.04 0.47 ng/uL 187151 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 entative ID MW MolForm CAS# Qual

1 Cyclohexane , methyl- 98 C7H14 000108-87-2 97 2 Cyclohexane , methyl- 98 C7H14 000108-87-2 96 3 Cyclohexane, methyl- 98 C7H14 000108-87-2 96 4 3-Pentin-2-one, 4-methyl- __________ 98 C6H10O 000141-79-7 52 Abundance C Scan 22 (5.040 min): 26986.D (-) m/z 83.05 100.00% ; 55 83 41 5000- 98 69

miz-> +51 ' i" '' i1' ■11" " i ■ — l — + 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m/ z 55.10 80.68% 'Abundance #63236: Cyclohexane, methyl- 55 83 — 5000 98 T’T 42 4.90 5.00 5.10 5.20 5.30 5.40 5.50 27 m/z 41.05 70 i 50.83% i ‘ TTTTTTTT ■ i111' i' ■111' ■ i'11' 11 ——— 6611 ' i ■ " ' r ■' r m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1326: Cyclohexane, methyl- 55 83 A I'' ’' I *' ’ ‘ I TOTT 4.90 5.00 5.10 5.20 5.30 5.40 5.50 5000 98 m/z 98.05 41.44% 42 27 69

' i ■ ■' • i ■i1" • i' ■'' i" ■' r 1" i' " ' i " ■' i ■ ■ ■' i11 ■ ■ i' " ' i' ■ ■ ■ i ■ ■1 ■ i''' ■ i' ■ ■' i' " ' i'' " I*' m/z--> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 \ 'Abundance #63235: Cyclohexane, methyl- ■ * I ’''' I ’''' I *''' I'' '' I 55 83 4.90 5.00 5.10 5.20 5.30 5.40 5.50

.N m/ Z 33.81% 5000- 98 42 69 27 ...I...... i""r‘ •r"•r•••i +TTP- +t i" " i mm T’T f m/z--> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 4.90 5.00 5.10 5.20 5.30 5.40 5.50

26986.D NP112701.M Tue Dec 11 14:51:19 2001 Page 1

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