GCMS results log, sample AD26985, Dec 11 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26986.D Vial: 32 Acq On 7 Dec 2001 3:19 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 l-Pentanol, 4-methyl- Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

5.15 0.59 ng/uL 233506 1,4-Dichlorobenzene-d4 11.89

Hit# Of 5 entative ID MW MolForm CAS# Qual

1 1-Pentam , 4-methyl- 102 C6H140 000626-89-1 36 2 1-Buta: 1 74 C4H10O 000071-36-3 33 3 Ethyl imine 43 C2H5N 000151-56-4 9 4 Cycl utane 56 C4H8 000287-23-0 9 Abundance Scan 34 (5.150 min): 26986.D (-) m/z 41. 05 100.00% 41 1 56 59

5000-

71 ■ ■ i ■ ■ <—i—|—>■ । ■ । । । । । i i । । 45 i11 ■' i ■11' i ■ ■ ■11''' ■ i'' ■'i■ —3l | ■ | ■ ■ • ■ ।1 53 + 67 T’r TITI TIVIEIIIT > ij . . .-i p-r ____5.00 m/z 56 5.20 5.40 81.40%| 5.60

miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #63578: 1-Pentanol, 4-methyl- 56 41 69 5000 T i ■ ■ • 1 3 —-—frr 5.00 5.20 5.40 5.60 m/ z 42 . 05 71.78% 45 I 159 | 84 i'111r' ■11'' ■1 r '" i ■1'' i' ■ ’' i"'11 -r-fT-rn-j-r •| ‘|■i • ■" I • ■ • ■ i • i ■■’'i■•" i ■ m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 7C 75 80 85 90 Abundance #62584: 1-Butanol 41 56 । i । ' ' i-r । ' 1 ′ T "i 5.00 5.20 5.40 5.60 5000 m/z 59. 10 69.70%

45 I 38 53 I ‘1‘1111——"tT‘rrr11—E11—T9I61EEIETTSIG-GIITISTTTr l i''1' i''1' r ■ ■' r " ' i'' ■ ■ i ■'' ■ r '1' i' m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 'Abundance #62261: Ethylenimine 42 5.00 5.20 5.40 5.60 m/ z 43 . 05 61.11% I 5000-

m/z--> 5 15

TTTTTTTT • • i • • n i + T . .—I ■ । 10 15 20 25 27

30 35 39

40 ' ।' 45 »i ■ ■ • ■ i' ■ • ■ i • ■ • ■ i ■ • ■ ■ i' ■ • ■ i ■ ■ •' i • ■ ■ * I ■ ’1 ■ i • 50 55 60 65 70 75 80 85 90 J 5.00 5.20 5.40 5.60

26986.D NP112701.M Tue Dec 11 14:51:21 2001 Page 2

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