GCMS results log, sample AD26847, Dec 11 2001

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Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26847. D Vial: 23 Acq On 7 Dec 2001 6:10 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1,00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C : \DATABASE\NBS75K. L ********************************************************************* Peak Number 1 Cyclohexane, methyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

5.06 0.4 5 ng/u: 188658 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclohexane, methyl- 98 C7H14 000108-87-2 97 2 Cyclohexane, methyl- 98 C7H14 000108-87-2 96 3 Cyclohexane, methyl- 98 C7H14 000108-87-2 95 4 lH-Pyratole, 4,5-dihydro-4,5-dimeth 98 C5H10N2 028019-94-5 64 Abundance 7 Scan 23 (5.056 min): 26847.D (-) m/ z 55.10 100.00% 55 83

41 98 5000- 69 TT 4ff TTT

m/z-> 20 "I ’11' I' 1111 " 11 " 25 30 35 40 1.... 514 - 45 50 55 60 65 70 75 80 85 —d —TTT 90 95 100 105 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m/ z 83.05 97.06% Abundance #63236: Cyclohexane, methyl- 55 83

5000- 98 » ‘ 'i TT 42 4.90 5.00 5.10 5.20 5.30 5.40 5.50 27 70 m/z 98.15 53.16% 661 1' i ’'111''1 ■ i ■ ' i'''' i ■ fur m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63235: Cyclohexane, methyl- 55 83 I'''' f r•••i

u. 4.90 5.00 5.10 5.20 5.30 5.40 5.50 5000 98 m/ z 41.00 49.31% 42 69 27 TTTTTTTTPuu)——upmeum“"umoritr m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 'Abundance #1326: Cyclohexane, methyl- 4.90 5.00 5.10 5.20 5.30 5.40 5.50 | 55 83 m/ z 42.10 36.46% 5000- 98 42

M__ 27 69

Im/z-> ' i ■ ‘ " i' TTT TT " i' “ ' i " ............... — — + T’TTTT J ‘‘ ‘‘ I w 4444 , 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 4.90 5.00 5.10 5.20 5.30 5.40 5.50

26847.D NP112701.M Tue Dec 11 14:48:06 2001 Page 1

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