GCMS results log, sample AD26988, Dec 11 2001

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Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26988.D Vial: 15 Acq On 6 Dec 2001 10:54 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclohexane, methyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

5.04 0.57 ng/uL 207798 1,4-Dichlorobenzene-d4 11.88

Hit# of 5 Tentative. ID MW MolForm CAS# Qual

1 Cyclohexane, methyl- 98 C7H14 000108-87-2 97 2 Cyclohexane, mechyl- 98 C7H14 000108-87-2 95 3 Cyclohexane, methyl- 98 C7H14 000108-87-2 94 4 1H-Pyrazole, 4,5-dihydro-4,5-dimeth 98 C5H10N2 028019-94-5 64 Abundance Scan 22 (5.044 min): 26988.D (-) m/z 83.05 100.00% 55 83

41 5000 - 98 69 P t I I | t ! I ! | ! I I l| I IM |

miz-> 20 — TTIVPBpannrT-rrrrTT , Tht 25 30 35 40 45 50 55 60 65 70 , 51 + ■ i ■ " ' i • ITT h....... 75 80 85 90 95 100 105 4 90 5.00 5.10 5.20 5.30 5.40 5.50 m/ Z 55.10 97.82% Abundance #1326: Cyclohexane, methyl- 55 83i TPTA —IPI 5000- 98 42 4.90 5.00 5.10 5.20 5.30 5.40 5.50 27 69 m/ z .41.05 50.33% 52

_A " r ■ ■ ■ i' TTTT-ri- ■ • I ■' ■ ’ I ■ • ■ • I' .JI TIT TTT 11'1'11' i""l 1 I'''1I m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 'Abundance #63236: Cyclohexane, methyl- 55 83 1 ■ i'1 4.90 5.00 5.10 5.20 5.30 5.40 5.50 5000 98 m/z 98.05 43.29% 42 27 70 66 TTTTI’ITTT ■ i ■ ■. ■ i ■ ■ ■ > l ‘ i1'1 ■ i'1 ■' i' ■ ■' i''' ■ i ■1'' i m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63235: Cyclohexane, methyl- I‘ ’I''*'I ''‘'I'‘ 'I 55 83 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m/ Z 42.00 35.35%

A_ 5000 98 42 69 27 I I - ■ i" " i1' ■ I " T‘1'' TTTTTTT TT" ....... 11' ■ " i ■' 'T'" • 1f 11 « . > । । - m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 4.90 5.00 5.10 5.20 5.30 5.40 5.50

26988.D NP112701.M Tue Dec 11 14:53:34 2001 Page 1

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