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GCMS comments for sample AD26473 detecting N,N-dimethylbenzenesulfonamide

Machine-extracted title · confidence 100%

DEP lab report dated December 10, 2001, identifying N,N-dimethylbenzenesulfonamide at 0.49 ug/L in sample AD26473.

NYC-WTC_000031636–000031649

Folder label: “GCMS X 11/5/01 A 12/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26473.D Vial: 9 Acq On : 30 NOV 2001 7:30 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclohexane, methyl- Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 5.04 0.50 ng/uL 210151 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclohexane, ethyl- 98 C7H14 000108-87-2 97 2 Cyclohexane,/methyl- 98 C7H14 000108-87-2 97 3 Cyclohexane/ methyl- 98 C7H14 000108-87-2 97 4 1H-Pyrazol/, 4,5-dihydro-4,5-dimeth 98 C5H10N2 028019-94-5 72 Abundance Scan 22 (5.041 min): 26473.D (-) m/z 83.05 100.00% 55 80

5000 41 98 69 51 1 1 4.90 5.00 5.10 5.20 5.30 5.40 5.50 it 111TT 111 j 111111 i 11 t H[mmh - m1 - mImp]mgt 94 m/z 55.10 91.27% mz-> Abundance 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 #63235: Cyclohexane, methyl- 55 83

5000 98 42 4.90 5.00 5.10 5.20 5.30 5.40 5.50 69 m/z 41.05 47.96% 27

JU m : > ] 111 > ] 11 11 - ! 11111 > 111 rl- - m Hmm mm mz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1326: Cyclohexane, methyl- 83 55 111111111111TTII 11.' l.. " I ■ •. • 111 4.90 5.00 5.10 5.20 5.30 5.40 5.50 5000 98 m/z 98.15 44.55% 42 27 69

111"' > i1 m m ■ H+ ' m H 11" ■11 ■"1 miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 ... \.............. Abundance #63236: Cyclohexane, methyl- 1111111 ।••••। . i • • • • i" • • i • • 55 83 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m/z 56.10 35.86% 5000

m/z—> 27 42

111"1111 4 4 ' +641 - - H H 20253035404550556065 70 75 80859095 100105 70 98

_N__ TITEgTa 4.90 5.00 5.10 5.20 5.30 5.40 5.50

26473.D NP112701.M Tue Dec 04 10:45:12 2001 Page 1

NYC-WTC_000031642

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