GCMS analysis report for sample AD26471, Dec 2001

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26470.D Vial: 23 Acq On : 1 Dec 2001 8:12 am Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise 2 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclohexane, methyl- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 5.05 0.41 ng/uL 194296 1,4-Dichlorobenzene-d4 11.89

Hit# Of Tentative ID 5 MW MolForm CAS# Qual 1 Cyclohexane, methyl- 98 C7H14 000108-87-2 96 2 Cyclohexane, methyl- 98 C7H14 000108-87-2 94 3 Cyclohexane,/methyl- 98 C7H14 000108-87-2 94 4 1H-Pyrazole/ 3-ethyl-4,5-dihydro- 98 C5H10N2 005920-29-6 58 Abundance 4 Scan 23 (5.051 min): 26470.D (-) m/z 83.05 100.00% 55 83

41 98 5000 69 .A । । : I i b । i : i i । I i > < । i i 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m + ■ +74 " Hl ■ mAG ■ - m m/z 55.10 96.81% mz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1326: Cyclohexane, methyl- 83 55

5000 98 10 42 4.90 5.00 5.10 5.20 5.30 5.40 5.50 27 m/z 41.00 53.87% 69

—m juL " I 1,1 1 I ' TIITTI’ fpur T-rp-rrrprrr +1111" I 99111411

m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63236: Cyclohexane, methyl- 55 83

4.90 5.00 5.10 5.20 5.30 5.40 5.50 5000 98 m/z 98.05 48.23% 42 27 70 111 “11 — mmmm mmmm ‘ I 69 ' mmm ' H mz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63235: Cyclohexane, methyl- mmme 83 4.90 5.00 5.10 5.20 5.30 5.40 5.50 55 m/z 56.05 34.38%

5000

nfe-> 27 42

mmm mp ' m# ‘ mmm Immm mmmm 69

20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 98

_AN A 1 A. I I JIT 4.90 5.00 5.10 5.20 5.30 5.40 5.50

26470.D NP112701.M Tue Dec 04 15:40:57 2001 Page 1

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