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GCMS results log, sample AD27007, Dec 11 2001

Machine-extracted title · confidence 100%

Laboratory report for GCMS analysis of sample AD27007 completed on December 11, 2001.

NYC-WTC_000032503–000032519

Folder label: “GCMS X 11/8/01 A 12/7/01”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\27007.D Vial: 22 Acq On 7 Dec 2001 5:16 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclohexane, methyl- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

5.03 0.60 ng/uL 200657 1,4-Dichlorobenzene-d4 11.89

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclohexane, ethyl - 98 C7H14 000108-87-2 97 2 Cyclohexane , ethyl- 98 C7H14 000108-87-2 95 3 Cyclohexane, methyl- 98 C7H14 000108-87-2 94 4 1H-Pyrazole, 4,5-dihydro-4,5-dimeth 98 C5H10N2 028019-94-5 64 Abundance Scan 20 (5.025 min): 27007.D (-) m/z 55.10 100.00% 55 83

41 • 5000- 98 69 T‘ 4.90 5.00 5.10 5.20 5.30 5.40

m/z-> 20 25 30 HT -m -d 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 f, TT TTT TTTTTTIWTTTTTT m/ z 83.05 95.78% Abundance #1326: Cyclohexane, methyl- — 0 83

5000- 98 T III i' •'' i' ■'' i TT 42 4.90 5.00 5.10 5.20 5.30 5.40 27 69 m/z 41.10 50.96% ... 1......1 "18 TFTTTTTTTTTT‘E-‘I-TTIT-IIIIII"I1" 90 TTTTTTTTTTTTT m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 95 100 105 Abundance #63236; Cyclohexane, methyl- I 55 83 TTT TT i-ri । i i i i । , i i i । TIT 4.90 5.00 5.1' 5.20 5.30 5.40 5000 - 98 m/ z 98.05 44.07% 27 42 70 ____________ 66__________ ____________________ ■ i' "' i ■ ■1' r "11'' " i'1 •' r " ■ ।'. ■ ■ । ■ >' ■ ।" 1' i " 1' i " '' i " •' r ' m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63235: Cyclohexane, methyl- - 55 83 4 90 5.00 5.10 5.20 5.30 5.40 m/z 56.10 30.96% 5000- 98 42 69 27

m/z-> I TTTTTTTTTTTTT 20 25 30 T’TTTT T-rp- mmTTTT 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 + TTT ' 11''' 11' AAM— 4.90 5.00 5.10 5.20 5.30 5.40

27007.D NP112701.M Tue Dec 11 14:56:42 2001 Page 1

NYC-WTC_000032511

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NYC-WTC_000032511Source: NYC Law Department, mirrored locally

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