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GCMS results log, sample AD27009, Dec 11 2001

Machine-extracted title · confidence 100%

Laboratory report for GCMS analysis of sample AD27009 completed on December 11, 2001.

NYC-WTC_000032534–000032552

Folder label: “GCMS X 11/8/01 A 12/7/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\27009.D Vial: 28 Acq On 7 Dec 2001 11:38 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclohexane, methyl- Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

5.05 0.4 5 ng/uL 227146 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 entative ID MW MolForm CAS# Qual

1 Cyclohexane, methyl- 98 C7H14 000108-87-2 95 2 Cyclohexane, methyl- 98. C7H14 000108-87-2 95 3 Cycl hexane, methyl- 98 C7H14 000108-87-2 95 4 1H-P razole, 4,5-dihydro-4,5-dimeth 98 C5H10N2 028019-94-5 64 Abundance ‘ Scan 23 (5.052 min): 27009.D (-) m/z 83.05 100.00% 55 83

41 98 5000 69 i ■ ■' ■ i TTI‘"E‘1‘171111110111IT 4.90 5.00 5.10 5.20 5.30 5.40 5.50

m/z~> — -----511 1TT T TTTTTTT ■7-^ 20 25 30 35 4G 45 50 55 60 65 70 75 80 85 90 95 100 105 U m/z ,55.10 96.47% Abundance #63235: Cyclohexane, methyl- I I 55 83 i — 5000- 98 11 42 4.90 5.00 5.10 5.20 5.30 5.40 5.50 69 m/ Z 41.00 50.03% 27 1 ' ' I ' ' ' ' I ’ TTTTTTTTTTTTTT 1 r " ■ ।•' 111 ........ 1" m/z-> 'Abundance I I 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 #63236: Cyclohexane, methyl- 5.5 8.3 W l ■ ■ ■ ■ l ■ ■ ■ ■ l ■ ■ • • I ■... I, TTTTIur 4.90 5.00 5.10 5.20 5.30 5.40 5.50 5000- 98 m/z 98.05 43.92% 42 27 70 66 r■"I" m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1326: Cyclohexane, methyl- I'''' I ’''' I i ■ > ■ ■ i ■ ■ I 55 83 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m/ Z 42.00 33.76% 5000- 98 42 27 69

m/z-> ‘I‘ r ''' I i' ■ ■' i trpt IPT • | ‘ ' I " 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 m X A A I ’ 4.90 5.00 5.10 5.20 5.30 5.40 5.50 ,-rr-rj-rm-p-r

27009 .D NP112701 .M Tue Dec 11 14:59:22 2001 Page 1

NYC-WTC_000032541

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NYC-WTC_000032541Source: NYC Law Department, mirrored locally

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