GCMS calibration table for TCLP analysis, Dec 6 2001

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Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\LBB.D Vial: 14 Acq On 6 Dec 2001 10:00 pm Operator: GALOS Sample lab blank 11/8 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table .Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 3-Hexanone Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

6.48 0.46 ng/uL 170042 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanone 100 C6H120 000589-38-8 91 2 3-Hexanone' 100 C6H120 000589-38-8 91 3 3-Hexan ne 100 C6H120 000589-38-8 78 4 Butane/ 2,2-dimethyl- 86 C6H14 000075-83-2 42 Abundance Scan 179 (6.485 min): LBB.D (-) m/z 43.05 100.00% 43 57

71 5000 100 39 6.20 6.40 6.60 6.80 mm + 1WTTH T’T’TTTTTTT t I" " I m/z 57.10 88.59% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63358: 3-Hexanone 43 57

71 21* ' 1 5000 6.20 6.40 6.60 6.80 100 m/z 71.05 49.71% 85 m/z-> I'1111 I" " I " Hr II’ +n 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1 528: 3-Hexanone 43 57 A. 6.20 6.40 6.60 6.80 29 71 5000 m/z 100.05 31.15% 100 85 TI]WWTp—TTTummuuuuO"Bu3UT TrrnT m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance 43 #63356: 3-Hexanone .A...1.. —... - 29 57 6.20 6.40 6.60 6.80 m/z 41.10 23.37% 5000 71

100 38 , 85 —MAr......... ..... " • i" ‘' i' r • • • i •" • i 1 'I"......... I' "I'...... TIT " i" " r1" r TTTTTT 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.20 6.40 6.60 6.80

LBB.D NP112701.M Wed Dec 12 08:19:08 2001 Page 5

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