GCMS calibration table for TCLP analysis, Dec 6 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DECO6O1\LBB.D Vial: 14 Acq On 6 Dec 2001 10:00 pm Operator: GALOS Sample lab blank 11/8 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 6 2-Hexanone Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

6.59 0.50 ng/uL 186218 1,4-Dichlorobenzene-d4 11.89

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanone 100 C6H120 000591-78-6 /9 2 2-Hexanone 100 C6H120 000591-78-69 3 2-Hexanone 100 C6H120 000591-78-69 0 4 2-Hexanone, 4-hydroxy-3-propyl - 158 C9H1802 062338-17-4 83 Abundance Scan 191 (6.595 min): LBB.D (-) m/ z 43.00 100.00%! 43

5000-

।" " i " " । 11" " r I 71 58

100 85 mmmmTRTT — 11" " i 6.20 m/z N 6.40 58.10 6.60 6.80 7.00 55.69% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63384: 2-Hexanone I 43

5000 58 ----- -P ------------ 6.20 6.40 6.60 6.80 7.00 29 m/z 41.00 15.90% 39 100 I I ■ < i •11' (11 TTTTTTTTTTTT - r...... TOPPTTT TIM 71 85 m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63385: 2-Hexanone 43

6.20 6.40 6.60 6.80 7.00 5000 - 58 m/ z 57 05 15.45% 29 39 , 71 85 100 : PuuumimgTuuu i..,, t....,,.., P ,..,..,. ।। P । <! । > 111! m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105__ Abundance #1556:2-Hexanone TIII—RTT ; 43 6.20 6.40 6.60 6.80 7.00 m/z 100.15 9.93% 58 5000-

27 39 71 85 100

m/z-> TTTTTTTTTTTTT tmmm 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.20 6.40 6.60 6.80 7.00

LBB.D NP112701.M Wed Dec 12 08:19:10 2001 Page 6

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