Calibration data sheet listing standard compounds and response factors used for GCMS analysis on December 6, 2001.
NYC-WTC_000032269–000032285Folder label: “GCMS X 11/8/01 A 12/7/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\l\DATA\DEC0601\LBB.D Vial: 14 Acq On 6 Dec 2001 10:00 pm Operator: GALOS Sample lab blank 11/8 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L
Peak Number 7 2-Butanol, 3-methyl- Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T.
7.18 1.3 6 ng/uL 504398 1,4-Dichlorobenzene-d4 11.89
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 2-Butanol. 3-methyl- 88 C5H120 000598-75-4 38 2 2,3-But nediol 90 C4H10O2 000513-85-9 28 3 Ethane,/ 1,1-diethoxy- 118 C6H1402 000105-57-7 9 4 Ethane, 1,1-diethoxy- 118 C6H1402 000105-57-7 9 Abundance Scan 255 (7.182 min): LBB.D (-) m/z 45.00 100.00% 45
5000- 61 73 A 6.80 7.00 7.20 7.40 7857 । , m/z-> TTTTTTETTTTTTT’T 88 IIT rh n lmmH l!l 111 207 1'11 ■ i 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 m/ z 43.00 83.37% 'Abundance #62961: 2-Butanol, 3-methyl- 45
5000 1“k | ' ■ 1 ' | ■
6.80 7.00 7.20 7.40 7.60
55 73 m/z 61.00 32.99% 27 I 87 1 , m-ry 11.111 •. 1. 111111111. (! I. • 111 •. 11 M 111 • 11 p n rp n 11 ri. 11 I " ■1 r Ti I' ’" I' ’ ” I m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance #917: 2,3-Butanediol 45
6.80 7.00 7.20 7.40 7.60 5000 m/z 73.05 3 0.23% 29 19 57 i I ■' >' I ■ •»■ I ■'" I 75 90 m/z-> i""r I"'111 ’" 11"111'111'" ’ 111'111'" 11 ’111" " I"1' 11'" I"1 • I' 11'111 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 A 4 Abundance
5000 - #64434: Ethane, 1,1-diethoxy- 45
73 m/z 70_T 6.80 7.00 7.20 7.40 7.60
1527 TTTTTTTTPT : i J 61 , i i. j it i i |M 89 103 | 1.1111111 l'l I ‘T’TTTTTTTTTTTTTTT P.. I I I I I I I I I I I I I I I I I I i t m/z-> 10 20 30 40 50 60 70 80 90 100110 120130140150160170180 190 200 21G 6.80 7.00 7.20 7.4G 7.60
LBB.D NP112701.M Wed Dec 12 08:19:12 2001 Page 7
NYC-WTC_000032281
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NYC-WTC_000031665
Instrument output file listing calibration standards and response factors for various compounds used in the December 7, 2001 analysis.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031685
Analysis report dated December 16, 2001, stating that mass spectrometry of sample AD26475 revealed no non-target compounds.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031707
Analysis report dated December 16, 2001, stating that mass spectrometry of sample AD26476 revealed no non-target compounds.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031876
Calibration table listing standards like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 for GC/MS analysis dated December 2001.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031739
Analysis report dated December 16, 2001, stating that mass spectrometry of sample AD26478 revealed no non-target compounds.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000032182
Laboratory report documenting GCMS analysis of sample AD26828 identifying unknown compounds on December 10, 2001.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031452
Report documenting GCMS analysis of sample AD26388 with a note regarding unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031509
Analysis report for sample AD26391 indicating the presence of other unknown compounds on December 4, 2001.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031433
Report documenting GCMS analysis of sample AD26387 with a note regarding unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031847
Mass spectrometry analysis of sample AD26537 found no non-target compounds present, Dec 16, 2001.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000032343
Laboratory report for GCMS analysis of sample AD26982 completed on December 11, 2001, noting unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031831
Analysis report dated December 16, 2001, identifying 1,1,2,2-Tetrachloroethane at 3.2 ug/L in sample AD26536.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000032266
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000032267
Fragmented header page from a GCMS data file associated with the December 7, 2001 testing period.
Filed in the same folder
NYC-WTC_000032286
Laboratory report for GCMS analysis of sample AD26833 completed on December 11, 2001, showing surrogate recovery data.
Filed in the same folder
NYC-WTC_000032308
Laboratory report for GCMS analysis of sample AD26845 completed on December 11, 2001, indicating unknown compounds.
Filed in the same folder
NYC-WTC_000032321
Laboratory report for GCMS analysis of sample AD26346 completed on December 11, 2001, with surrogate recovery results.
Filed in the same folder