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GCMS analysis results for sample AD26711, Dec 10 2001

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Laboratory report documenting GCMS analysis of sample AD26711 identifying unknown compounds on December 10, 2001.

NYC-WTC_000032128–000032141

Folder label: “GCMS X 11/7/01 A 12/6/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0501\26711.D Vial: 5 Acq On 5 Dec 2001 12:24 pm Operator: GALOS Sample gc/ms unknown 11/7 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 2-Butanol, 3-methyl-, (S)- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.19 8.78 ng/uL 3110250 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Butanol, 3-methyl- , (S) - 88 C5H120 001517-66-4 42 2 2,3-Butane iol 90 C4H10O2 000513-85-9 33 3 2-Butanol, 3-methyl- 88 C5H120 000598-75-4 9 4 2-Butanol, 3-methyl- 88 C5H120 000598-75-4 9 'Abundance • Scan 256 (7.187 min): 26711.D(-) m/ z 4 5.10 100 . 00% i 45

5000 61 73 ( — - 6.80 7.00 7.20 7.40 7.60 —36 l4— 88 in ।... i।।।. TTTT 11111 > । ।. h । 207 TT '"i1 m/z 43.00 59.94% mz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #852: 2-Butanol, 3-methyl-, (S)- 45 । i — 5000- ' 1 1 1 1 1 1 1 1 6.80 7.00 7.20 7.40 7.60

55 73 m/z 73.05 36.64% 27 I |... 87 ITT "i" " i 1" " I " ' ‘ I '1 H I TT-rrrprrrpnT-TjTTTTpn^ miz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 210 'Abundance #917: 2,3-Bulanedio! 45 i-1 1 1 ' ‘ I ' 1 — 6.80 7.00 7.20 7.40 7.60 5000- m/ z 61.00 35.77% 29 19 57 I 75 90 TOTUT r " ■ i ■H' r ■" i I "" I " " i " " I ‘1" I " " r" 111I " " 11 ’ T i ■ ■' ■ i" " i' ■" i miz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 'Abundance #62961: 2-Butanol, 3-methyl- ■। > 4 7 । | I

45 6.80 7.00 7.20 7.40 7.60 m/ z 44.0.5 11.66% 5000

55 73 I" " I .... JI,,. JU T’’F I’L ’T 87 i" " i ■, . । । . < n j 'i i । i । i i m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 210 6.80 7.00 7.20 7.40 7.60

26711.D NP112701.M Fri Dec 07 13:14:32 2001 Page 2

NYC-WTC_000032136

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NYC-WTC_000032136Source: NYC Law Department, mirrored locally

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