GCMS analysis results for sample AD26711, Dec 10 2001

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Data File C:\HPCHEM\l\DATA\DEC0501\26711.D Vial: 5 Acq On 5 Dec 2001 12:24 pm Operator: GALOS Sample gc/ms unknown 11/7 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 Hydrogen azide Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

5.05 2.86 ng/uL 1011950 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hydrogen azide 43 HN3 007782-79-8 4 2 Acetic acid, anhydride 102 C4H603 000108-24-7 2 3 Acetic Acid, anhydride 102 C4H603 000108-24-7 2 4 Acetic acid ethenyl ester 86 C4H602 000108-05-4 2 Abundance Scan 23 (5.050 min): 26711.D (-) m/z 43.00 100.00%| 43

5000-

4.90 5.00 5.10 5.20 5.30 5.40 5.50 51 36 40,60 87 1 ‘ I |-n i i | ri rr ।i11111'11 ‘ i1 TTTTTTT’TTT +1 i'1111 r’ m/ z 42.00 6.01% miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #33: Hydrogen azide 43

5000 15 i • • • • i • ’1 • i 111 4.90 5.00 5.10 5.20 5.30 5.40 5.50 29 m/z .44.00 2.90% TT TIT | ' 1 1 1 | 1 I1 । i i I i । I i r, । ,, . ( । । ।।, I'"' 11 miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 'Abundance #1680: Acetic acid, anhydride 43 T’EEIEEEEII-TETT 4.90 5.00 5.10 5.20 5.30 5.40 5.50 5000 m/z 41.00 1.13%

29 I 1T TTTTTTTTTTT >.. ।.... । ITTTTTTETCTTTTTTTT87‘1‘‘‘111 TEE‘‘I"TETETTTTTT‘‘60 m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63470: Acetic acid, anhydride A N l * • ■ ■ I''. 11 ■I TTtT‘1r1‘r1 1"— i 43 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m/z 45.00 0.96% 5000-

15 ....J..... 29.... ! * 60 ■ i•■■■i■■•<I"•■i"'■i'i "i■ • • ■ i■1 87 111111 T‘ m/z-> 5 10 15 20 25 30 35 4G 45 50 55 60 65 70 75 80 85 90 95 4.90 5.00 5.10 5.20 5.30 5.40 5.50

26711.D NP112701.M Fri Dec 07 13:14:30 2001 Page 1

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