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GCMS analysis results for sample AD26681, Dec 10 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD26681 identifying unknown compounds on December 10, 2001.

NYC-WTC_000032079–000032092

Folder label: “GCMS X 11/7/01 A 12/6/01

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Scanned page image, NYC-WTC_000032084
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0401\26681.D Vial: 2 Acq On 4 Dec 2001 11:44 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 Hydrogen azide Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

4.98 1.09 ng/uL 461904 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hydrogen azide 43 HN3 007782-79-8 1 2 Acetic acid, anhydride 102 C4H603 000108-24-7 1 3 1,4-Benzenediol, 2,3-dichloro-5,6-d 312 C12H6C12N2O4 000000-00-0 1 4 Acetic/acid, anhydride 102 C4H603 000108-24-7 1 Abundance Scan 15 (4.982 min): 26681.D (-) m/z, 43.00 100.00% 43

5000-

1’ i • • • • i ■p-n-rj-rr 4.90 5.00 5.10 5.20 5.30 5.40 _66 TT . i , rpi 11 | i i r r | * I ■''' i ■ ■ ■ ■ i 1 ‘ • i1 ■ ■ ■ i'1 •11 11 11 'I I ■ •'' I r m/z 42 -00 5.34%

AN m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 'Abundance #33: Hydrogen azide 43

5000- 15 4.90 5.00 5.10 5.20 5.30 5.40 29 — m/ z 44.00 2.50% TIT TIT i • • • • I i • • ■ ■ i TT IT m/z-> 201 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #1680: Acetic acid, anhydride

0" 43 i' ’ ■ ■ i I 1 1 ' ' I' '

5000-

29 , 60 87 m/z--> Abundance .............. . 20 40

43 TI—TTTTT r 1’001110010011177 TT, , TIII——ImuOwtav 60 80 100 120 140 160 180 200 220 240 260 280 300 #44406:1,4-Benzenediol, 2,3-dichloro-5,6-dicyano-, diaceta AAAW__ 4.90 5.00 5.10 5.20 5.30 5.40 i m/z 41.00 0.48% 5000

87 109 200 228 270 312 TTTTTTTTT ‘I‘—"101ETt0‘‘""1‘‘‘II_11-Trt7rrrrrLi 11,1111 ‘1' 1'1" TTTTTTHT m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 I 4.90 5.00 5.10 5.20 5.30 5.40

26681.D NP112701.M Fri Dec 07 13:12:21 2001 Page 1

NYC-WTC_000032084

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NYC-WTC_000032084Source: NYC Law Department, mirrored locally

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