GCMS Analysis Report for Sample AD26337, Dec 2001

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Data File C:\HPCHEM\1\DATA\NOV3 001\26337.D Vial: 25 Acq Oh 1 Dec 2001 10:01 am Operator: GALOS Sample gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 Hydrogen azide Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

5.00 0.72 ng/uL 192533 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hydrogen azide 43 HN3 007782-79-8 2 2 Acetic acid ethenyl ester 86 C4H602 000108-05-4 2 3 Acetic acid ethenyl ester 86 C4H602 000108-05-4 2 4 anti-2-Apietoxyacetaldoxime 117 C4H7NO3 037858-07-4 1 Abundance Scan 17 (5.001 min): 26337.D (-) m/z . 43.00 100.00% 4b

5000-

4.90 5.00 5.10 5.20 5.30 5.40 36 , 57 94 T*TUUeuumuaanuptrrrp+

AWX t 111 ‘' I I” "I ""I" "I r4 ” i TI m/z 42.00 5.25% m/z-> 5 10 15 20 25 3C 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #33: Hydrogen azide 43

5000- 15 4.90 5.00 5.10 5.20 5.30 5.40 29 m/z , 44.00 3.41% I ' i" " i"' l‘ ’I 11 n . I r. n p r j i ri. । rm ।।। । i'1" r " ■ i" " r "' r " m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #62796: Acetic acid ethenyl ester 43 ( . , . . | . . . . | . d > h b l h ] i • • • • i 4.90 5.00 5.10 5.20 5.30 5.40 5000- m/z 36 . 00 0.72%

15 27 86 ‘ I 1’1 I" ” I “ ‘ • I । ivn ।.. r. । r.n । mu p । n 11 >. > । > 11 111। i ।. 111 • 111111 11

m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #654: Acetic acid ethenyl ester 1 1 H , | I , ‘II 43 4.90 5.00 5.10 5.20 5.30 5.40 C 4S . 00 0.58% 5000

15 27 86 -1............. 1 l p»।. p.». p 111 p».. p ।. 1111 •. p । TTTTTTTT TTTT 111"' i miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 I ' ' ' ' I 4.90 5.00 5.10 5.20 5.30 5.40 I' ' ' ' I

26337.D NP112701.M Fri Dec 21 14:28:46 2001 Page 1

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