GCMS comments for sample AD26476 showing no non-target compounds

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Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0701\26476.D Vial: 6 Acq On 7 Dec 2001 10:40 pm Operator: GALOS Sample gc/ms unknown 11/6 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 Hydrogen azide Concentration Rank

R.T. EstConc Area Relative to ISTD R.T.

5.00 1.80 ng/uL 645467 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hydrogen azide 43 HN3 007782-79-8 4 2 Acetic a id, anhydride 102 C4H603 000108-24-7 2 3 2 - Propanone, 1-hydroxy- 74 C3H602 000116-09-6 2 4 2 -Propanone, 1-cyc1opropy1- 98 C6H10O 004160-75-2 2 Abundance Scan 18 (5.005 min): 26476.D (-) m/z 43.00 100.00% 4b

5000 -

...... TT 4.90 5.00 5.1G 5.20 5.30 5.40 rrp j i I 1 I I rr.ip...It i i . I 36.44 1— 55 60 69 83 TTTtTT 98 TTTTTT m/z 42.00 7.14% m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #33: Hydrogen azide 43

5000 15 I ‘ • 1I ' • 1 ' I ' ' ' * I '' ’' I 'I""I 4.90 5.00 5.10 5.20 5.30 5.40 29 m/ Z 44.00 3.04% Tt r "11 +r I'‘‘1)'1'’I'‘ 'I | | " I t | . I » I | M ! I | . . . • |

m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #1680: Acetic acid, anhydride 43

4,90 5.00 5.10 5.20 5.30 5.40 5000- m/z 41. 0 1.90% l 29 I.60 87 rrp 11' " I I"1' I TTTTTTTTm m/z--> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #62553: 2-Propanone, 1-hydroxy- i > • ■ ■ i ■ ■ • ■ । 11' ■ ■11 413 4.90 5.00 5.10 5.20 5.30 5.40 m/z 55.10 1.54%

J 5000

15 31 74

n/z--> TTTT +++2Q. —37 + TPTTTTTTTTTTTT T1"' I |. - > । । ■ r r । । । t । TTAT 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 4.90 5.00 5.10 5.20 5.30 5.40

26476.D NP112701.M Thu Dec 13 11:20:37 2001 Page 1

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