GCMS comments for sample AD26478 showing no non-target compounds

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Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0701\26478.D Vial: 3 Acq On 7 Dec 2001 7:56 pm Operator: GALOS Sample gc/ms unknown 11/6 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************* * *********************** Peak Number 1 Hydrogen azide Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

4.99 1.63 ng/uL 476967 1,4-Dichlorobenzene-d4 11.88

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hydrogen azide 43 HN3 007782-79-8 4 2 Acetic acid ethenyl ester 86 C4H602 000108-05-4 2 3 2-Propanone, 1-hydroxy- 74 C3H602 000116-09-6 2 4 Acetic acid, anhydride 102 C4H603 __ 000108-24-7 2 Abunda nce Scan 16 (4.985 min): 26478.D (-) m/z. 43.00 100.00% 43

5000

36 49 55 60 83 94 4.90 5.00 5.10 5.20 5.30 5.40 ITTTmTmpmmmjmpm m/z 42.05 6.45% miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #33: Hydrogen azIde

5000 15 43

AN l • ■ • ■ I •' * ■ l •1 ■ • i1 • ‘ ■ l1 ■ 4.90 5.00 5.10 5.20 5.30 5.40 29 m/z 44.00 3.13% mpmmmmmmmmmmmmmmmmmmm miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #654: Acetic acid ethenyi ester 43 T I i tt. j j . » i । » i » i j ) » » i j 4.90 5.00 5.10 5.20 5.30 5.40 5000 m/z 41.00 1.36% 15 27 86 11111.1. i. 11. i,.!. h , ] I,,,!..,,,..., t, I, I,,, I T| h I r 1111111111111II111111 ri I > 111111| I n 11 m-| > nr 11 in miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #62553: 2-Propanone, 1-hydroxy- j' • • ■ l 11’211 TT 413 4.90 5.00 5.10 5.20 5.30 5.40 m/z 45.00 1.11% 5000

15 31 W. 74 miz-> TIMTTTTT —3—374 11 .<. .|..i 11., >.(1... ।. 1. 11. Ill,.. i> ।.,.. ।.... । n .1 |i,, I IOUmTpAA 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 4.90 5.00 5.10 5.20 5.30 5.40

26478.D NP112701.M Thu Dec 13 11:22:03 2001 Page 1

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