GCMS comments for sample AD26475 showing no non-target compounds

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Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0701\26475.D Vial: 5 Acq On 7 Dec 2001 9:45 pm Operator: GALOS Sample gc/ms unknown 11/6 Inst : GC/MS Ins ■ Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Hydrogen azide Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

4.99 1.63 ng/uL 456682 1,4-Dichlorobenzene-d4 11.88

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hydrogen azide / 007782-79-8 4 43 HN3 2 Acetic acid, anhydride 000108-24-7 2 102 C4H603 3 Acetic acid, /anhydride 000108-24-7 2 102 C4H603 4 1,4-Benzenediol, 2,3-dichloro-5,6-d 312 C12H6C12N204 000000-00-0 1 Abundance Scan 16 (4.985 min): 26475.D (-) m/ z 43.00 100.00% 43

5000- । T TTTTr

A TT’’II 4.90 5.00 5.10 5.20 5.30 5.40 , 49 55 83 ‘ I ' l""f i1"11" " i 3.44 98 UT i •"11 l"'' i" " r " ■ i ■ •" r ■■ m/ z 42.00 5.99% m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #33: Hydrogen azide 43

5000- 15 4.90 5.00 5.10 5.20 5.30-5.40 29 m/ z 44.00 2.68% ■ r "' r " .. I... i +TTTT i" "i m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #1680: Acetic acid, anhydride 43 T I ■ ■ •' I ! 4.90 5.00 5.10 5.20 5.30 5.40 5000 m/z 41.00 1.21% I I 29 miz--> TUUOUTTTT’ r 60 87 i" " i" " r ■" r ■" r'" i" " i 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 I"'' I"'11'111 f

Abundance #63470: Acetic acid, anhydride I ..1 > l . . > I I .... I I’E 43 4.90 5.00 5.10 5.20 5.30 5.40 m/z 45.00 1.06%

_N 5000-

15 60

m/z-> 5 ... +... —29... ... । HTt 87 1’’ TpTrqTTTTJ- 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 i ■■ "i" "i i 4.90 5.00 5.10 5.20 5.30 5.40 •A A

26475.D NP112701.M Thu Dec 13 11:19:24 2001 Page 1

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