GCMS Analysis Report for Sample AD26336, Dec 2001

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Report documenting GCMS analysis of sample AD26336 with a note regarding unknown compounds.

NYC-WTC_000031384–000031399

Folder label: “GCMS X 11/5/01 A 12/1/01”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\HPCHEM\1\DATA\NOV3001\26336.D Vial: 30 Acq On 1 Dec 2001 2:36 pm Operator: GALOS Sample gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Hydrogen azide Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 5.01 0.62 ng/uL 197601 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual l Hydrogen a de 43 HN3 007782-79-8 4 2 Acetic acid, anhydride 102 C4H603 000108-24-7 2 3 1, 4-Benzenediol, 2,3-dichloro-5, 6-d 312 C12H6C12N2O4 000000-00-0 1 4 Propane/ 2-nitro-_________________ 89 C3H7NO2 000079-46-9 1 Abundance Scan 19 (5.013 min): 26336.D (-) m/z 43.00 100.00% 43

5000 J TTnumauugun 4.90 5.00 5.10 5.20 5.30 5.40 m/z 42.00 6.29%

AW- miz-> 20 40 60 80 100 120 140 160 180-200 220 240 260 280 300 Abundance #33: Hydrogen azide 43

5000 15 ‘ I 4.90 5.00 5.10 5.20 5.30 5.40 29 m/z . 44.00 3.32%

miz-> Wt-p- 20 A60 80 100 120 140 160 180 200 220 240 260 280 300 r 40 1′1′1111111 i " ■ ■ i ‘ ‘ i ■ " ‘ i'' “ i “ " i ‘ ‘ ■ ■ i

Abundance #63470: Acetic acid, anhydride 43 i " ' ‘ i “ ■ i " " i " i ■ ■ " i " “ i 4.90 5.00 5.10 5.20 5.30 5.40 5000 m/z45.10 1.39%

15 129 60 87 ..(.... । r ...J... 1 I " " I “ " r ' “ I •11 11'1111 TTTr I r n I I 11111111111 1111 '11111 111 11 miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #44406:1,4-Benzenediol, 2,3-dichloro-5,6-dicyano-, diaceta ..... A... I' ■'11'' ■ ‘ i ■'' ■ r ■ • ■ i • ■ ■' i • ■'11 43 4.90 5.00 5.10 5.20 5.30 5.40 m/z41.10 1.09% 5000

^iz-> 87 109 428 270 312 T-r-p- TTIT i11 ’11n “ I * ’ * ‘ i “ “ i11 “ i ’ ‘ IIITE0’ 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 200 111... ।. .ii 111 > 1111 i'i 11 UN i1 ■ “ i''1 ■ i “ ■ • i ‘ 4.90 5.00 5.10 5.20 5.30 5.40 “ i ■ “ ‘ i Ti

26336.D NP112701.M Tue Dec 04 15:07:49 2001 Page 2

NYC-WTC_000031393

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NYC-WTC_000031393Source: NYC Law Department, mirrored locally

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