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GCMS analysis results for sample AD26678, Dec 10 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD26678 identifying unknown compounds on December 10, 2001.

NYC-WTC_000032007–000032027

Folder label: “GCMS X 11/7/01 A 12/6/01

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Scanned page image, NYC-WTC_000032015
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0401\26678.D Vial: 4 Acq On 4 Dec 2001 1:33 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Hydrogen azide Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

4.98 1.37 ng/uL 378887 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hydrogen azi .e 43 HN3 007782-79-8 4 2 Acetic acid, anhydride 102 C4H603 000108-24-7 1 3 1,4-Benzenediol, 2,3-dichloro-5,6-d 312 C12H6C12N2O4 000000-00-0 1 4 Ethanamine, 2-methoxy-___________ 75 C3H9NO 000109-85-3 1 Abundance / Scan 15 (4.977 min): 26678.D (-) m/z 43.00 100.00%

J #3

5000

I' ' ' ’ I i • ■ • ■ i ■ 4.90 5.00 5.10 5.20 5.30 5.40 I , ..... A...... . i' ‘ •'[•••• i' >. 11. । . 11... 111.11 .. 111. • 11 I ‘' I V m/ z 42.00 5.60%

AN m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 'Abundance #33: Hydrogen azide 43

5000 15 I 1 ' 1 ‘ i ' 1 1 1 I ' 1 1 ' I 1 1 1 1 TTTT 1 4.90 5.00 5.10 5.20 5.30 5.40 29 m/ Z 44.00 2.68% ‘I" TPTIITI i ■ • i miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 'Abundance #1680: Acctic acid, anhydride 43 I , l r, l I ' 1 ' ' 1 1 ' ' ' 1 1 • • 1 I 4.90 5.00 5.10 5.20 5.30 5.40 5000- m/z 4 5.00 0.99%

m/z-> Abundance 29 1 . TTTTTIT 20 40

4)3 60 87 I ''' * I' ‘1' i * ‘' I I'' *' I •' 60 80 100 120 140 160 180 200 220 240 260 280 300 ' I' •'' 111111

#44406: 1,4-Benzenediol, 2,3-dichloro-5,6‘dicyano-. diaceta IT

AM 4.90 5.00 5.10 5.20 5.30 5.40 m/z 41.00 0.78% 5000

87 109 200 228 270 312 ■ ।' ■ ■ ■ । I ’'' 1 I T—TTT1 ■ | I . I ! | . I > . | I I| I ' 1 1 1 1 Tor 1 1 ‘ • I 1 1 ' 1 I TTrr m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 4.90 5.00 5.10 5.20 5.30 5.40

26678.D NP112701.M Fri Dec 07 13:08:35 2001 Page 1

NYC-WTC_000032015

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NYC-WTC_000032015Source: NYC Law Department, mirrored locally

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