GCMS Analysis Report for Sample AD26337, Dec 2001

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Data File C:\HPCHEM\1\DATA\NOV3 001\26337.D Vial: 25 Acq On 1 Dec 2001 10:01 am Operator: GALOS Sample gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Cyclobutane Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

5.16 1.10 ng/uL 294963 1,4-Dichlorobenzene-d4 11.89

Hit# of .5 Tentative ID MW MolForm CAS# Qual

1 Cyclobut ane/ 56 C4H8 000287-23-0 9 2 Guanidine / 59 CH5N3 000113-00-8 5 3 2-Butene, (E) - 56 C4H8 000624-64-6 5 4 Ethylenamine 43 C2H5N 000151-56-4 5 'Abundance Scan 34 (5.157 min): 26337.D (-) m/z 41.10 100.00% 41

5000

’ ’1’11’1111/11111111111" 36— TII 56 59

14 49 | 67 ----- ■ • i ■ ■ ■ ■ । 71 WA _ ----- MY III l r

m/z 5.00 5.20 5.40 5.60 74.14% m/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 Abundance #62310: Cyclobutane 41 56

5000 27 5.00 5.20 5.40 5.60 m/z 56.10 69.83%

WA - 38 49 53 | TTTT ‘U3 11I Tir i • i • • • > i > ■ ■ • i • • ■ > | ‘ ■ i miz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 Abundance #100: Guanidine 43 59

5.00 5.20 5.40 5.60

A 5000 m/z 42.05 58.16%

17 27 31 ._ i i 40 ’IT • • • । > i > ■ • ■ . ............. ' I ‘ ' I ' ' TT < > > . | i l ( . | > l > . | "I ■ . . | ! TT-J- m/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 Abundance #62302: 2-Butene. (E)- AAA 41 5.00 5.20 5.40 5.60 m/ 43.05 52.97% 56 5000 27 49 52 , miz-> ' I ' ' * ' I ' ' ‘ ‘ I ' 10 15 20 — 30... 34 I ++ 25 30 35 40 45 50 55 60 T-f ! . . r-p-m-j i i : i j T-m-r 65 70 75 80 5.00 5.20 5.40 5.60

26337,D NP112701.M Fri Dec 21 14:28:48 2001 Page 2

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