GCMS analysis results for sample AD26319, Dec 2001

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Library Search Compound Report

Data File C: \HPCHEM\1\DATA\DEC0501\25319 .D Vial: 7 Acq On 5 Dec 2001 2:13 pm Operator: GALOS Sample gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title 208 625/TCLP calibratio. table Library C: \DATABASE\NBS75K.L ******************************** ************************************ Peak Number 2 Cyclobutane Concentration Rank 14

R.T. EstConc Area Rolative to I STD R.T.

5.16 0.51 ng/uL 156251 1,4- ichlorobenzene-d4 11.87

Hit# Of 5 ntative ID 1W MolForm CAS# Qual 1 Cyclobutane 6 C4H8 000287-23-0 25 2 1-Propene, 2-methyl- 6 C4H8 000115-11-7 17 3 Oxirane/ trimethyl- ,6 C5H10O 005076-19-7 9 4 1 -Aziridineethanol "7 C4H9NO 001072-52-2 9 Abundance Scan 35 (5.165 min): 26319. D (-) m/z 41.10 100.00% 41 56 59

5000- 71 I 45 5.00 520 5.40 5.60

m/z-> 15 20 25 30 35 38 L 40 51 45 50 55 60 65 10 ■'1 ‘ t • • ■ ।«• ■ • । 70 75 9 . 11. ।. i j . ।.. ।. । 85 90 m/z 56.10 74.22% Abundance #62310: Cyclobutane 41

WW 56 I 5000- 27 500 5.20 5.40 5.60 m/z 43.10 72.21% 38 49 53 TPITT -TT

N ■' i'1'' i ■ m/z-> 15 20 25 30 35 40 45 50 55 '' 60 ' 65” 70 '' 75 085 90 Abundance #62306: 1-Propene, 2-methyl- 41

5.00 5.20 5.40 5.60 56 m/z 59.10 67.58% 5000 1

27 33 , 49 53 ,.. । -..111.. । "It **I m/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 0 85 90 Abundance #728: Oxirane, trimethyl- ---IT — 43 58 5.00 5.20 5.40 5.60 m/z 4 2.05 61.40% i\

5000 27

31 38 71 86 —1+ TItrurr TT 4 TITtma ■1'" ।"11111'11 A A AA m/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 0 85 90 5.00 5 20 5.40 5.60

26319 .D NP112701.M Wed Dec 05 15 :( :31 2001 Page 2

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