GCMS analysis results for sample AD26319, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C : \HPCHEM\1\DATA\DEC0501\25319.D Vial: 7 Acq On 5 Dec 2001 2:13 pm Operator: GALOS Sample gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P ■Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclohexane, methyl- Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

4 . 98 0.53 ng/uL 164351 1,4 -ichlorobenzene-d4 11.87

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclohexane, methyl- 18 C7H14 000108-87-2 95 2 Cyclohexane, methyl- 18 C7H14 0.00108-87-2 58 3 IH-Pyrazple, 4,5-dihydro-4,5-dimeth 98 C5H10N2 028019-94-5 53 4 2-Pentyne, 3,4-dimethyl-, (E)-______ 98 C7H14 004914-92-5 53 Abundance Scan 15 (4.981 min): 26319.D (-) m/z 55.10 100.00% 55 83

41 5000- 98 — 69 TTTmr li 111 ' ■ I 4.90 5.00 5.10 5.20 5.30 5.40 ’ ’IT rni IT .1,. r++ ‘ T‘ -74 TII80’ 4 511

85 1.) 95 100 105 ‘ ITT ' 11'" I ■ ■ m/z 83.05 99.49% m/z->_____ 20 25 30 35 40 45 50 55 60 65 70 75 Abundance #1326: Cyclohexane, methyl- 55 83

5000- 98 _— A ............... 42 4.90 5.00 5.10 5.20 5.30 5.40 27 69 m/ z 41.05 56.57%

i ■1 ’ 'i • *“ i TT 4.*p TTUTTTItr

_NN m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 180 85 0 95 100 105 Abundance #63234: Cyclohexane, methyl- i 55 83 I' ■ ■ ■ l 4.90 5.00 5.10 5.20 5.30 5.40 5000 m/z 98.05 47.54% 42 98 69 27 - T++ T-p-T ‘ I ' " ' I ' '

m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 i J 95 100 105 Abundance #1232: 1H-Pyrazole, 4,5-dihydro-4,5-dimethyl- ATII ,I ,| I ' ' ' 1 1 1 1 ' ‘ I 83 4.90 5.00 5.10 5.20 5.30 5.40 m/z 39.10 34.29%

U 5000 42 98

56 27 — - — :r 69 A 11<■ ■ ■ । ।• 11 T ITPIur I’ 1 ' I1 1 n/z-> 20 25 30 35 40 45 50 55 -60 65 70 75 80 35 ) 95 100 105 4.90 5 00 5.10 5.20 5.30 5.40

26319.D NP112701.M Wed Dec 05 15:( /:30 2001 Page 1

N YC- WTC_000031304