GCMS results log, sample AD27010, Dec 11 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0701\27010. D Vial: 34 Acq On 7 Dec 2001 6:06 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title 208 625/TCLP calibration table Library C: \DATABASE\NBS75K. L ********************************************************************* Peak Number 1 Cyclohexane, methyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

5.04 0.51 ng/uL 208115 1,4-Dichlorobenzene-d4 11.88

Hit# of 5 Tentative ID MW MolForm CAS# Qual

I Cyclohexane, methyl- 98 C7H14 000108-87-2 94 2 Cyclohexane, methyl- 98 C7H14 000108-87-2 94 3 Cyclohexane, methyl- 98 C7H14 000108-87-2 93 4 2-Pentene, 3,4-d imethyl - , (E) - 98 C7H14 004914-92-5 50 •Abundance Scan 22 (5.041 min): 27010.D (-) m/z 83.05 1 00.00% 56 83

41 5000- 98 69 / I ' 1 1 rl

++ lr i'1'11 4.90 5.00 5.10 5.20 5.30 5.40 5.50 T1H +514 +rpr 544— 36 , • r • " i' u1"' r1 m/ Z 55.10 96.77% miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63235: Cyclohexane, methyl- 55 83

5000- 98 AR f 4.90 5.00 5.10 5.20 5.30 5.40 5.50 42 69 m/z 41.05 58.43% : 27 i

i , I ii ' i1 ■ ■ ■ r "' i rp-

_WA m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63236: Cyclohexane, methyl- 55 83

4.90 5.00 5.10 5.20 5.30 5.40 5.50 5000- 98 m/z 98.05 44.90% 27 42 70 __________ __________ .. 66 _________: TTTTTTT ■ ■ ■ ■ | > > ■ • | < • • ■ | < < . ■ | • .-rf-rrrrp-n-Tj-r UIIICTIUTT’ T‘I0——————TTTTTEIITTT i > p-r m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1326: Cyclohexane, methyl- j . rr, । rr. TTTETTETETT 55 83 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m/ z ,56.10 38.62% 5000- 98 42 27 69

i

m/z-> < |i 11111 20 25 ‘IT I'1" I 30 35 40 45 50 -... 0 +t 55 60 65 70 75 80 85 90 95 100 105 i ■ ■ ■' i TTUIT’r i1 ’11 i AA Ir’r’ l 4.90 5.00 5.10 5.20 5.30 5.40 5.50

27010.D NP010302.M Wed Jan 09 12:22:01 2002 Page 1

NYC-WTC_000032561