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GCMS analysis results for sample AD26680, Dec 10 2001

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Laboratory report documenting GCMS analysis of sample AD26680 identifying unknown compounds on December 10, 2001.

NYC-WTC_000032058–000032078

Folder label: “GCMS X 11/7/01 A 12/6/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0401\26680.D Vial: 3 Acq On 4 Dec 2001 12:38 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title 208 625/TCLP calibration table Library C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclohexane, methyl- Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

5.00 0.84 ng/uL 226421 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclohexane,met hyl- 98 C7H14 000108-87-2 72 2 2-Pentene,3, 4-dimethyl - , (E) - 98 C7H14 004914-92-5 59 3 3 -Penten-2--one , 4-methyl- 98 C6H10O 000141-79-7 50 4 Cyclohexane, methyl - 98 C7H14 000108-87-2 45 'Abundance Scan 17 (5.001 min): 26680.D (-) m/ z 8’3.05 100.00% 56 83

41 98 5000 69 TPATT i • ■ • ■ i ■ • ■' । 4.90 5.00 5.10 5.20 5.30 5.40

m/z-> 5 "" i" i" " r"' i . . 4.. 'll 1C 15 2C 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 U TH m/ z 55.05 97.93% Abundance #63234: Cyclohexane, methyl- I

UA 55 83

5000 l • ■ r• l ■ ■ ■ ■ I ■ ■ ■ f l i ■ ■ ■ ■ l 4.90 5.00 5.10 5.20 5.30 5.40 42 98 69 m/z 41.05 51.82% 27 l .! I I I' • ’' I '1" I" " r ■" i ■ “' r ■ " r 1 1TTTTTTTTTTTTTTT m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #1362: 2-Pentene, 3.4-dimethyl-, (E)- 55 83

4.90 5.00 5.10 5.20 5.30 5.40 5000- m/ z 98.15 46.16% 27 98 15 69 42 50 | TTTTTTUTTTrr TPmgTTT p "‘I" " I” " I '"’I" "I

Abundance 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 #63217: 3-Penten-2-one, 4-methyl- —4 55 83 4.90 5.00 5.10 5.20 5.30 5.40

. L m/z 4 2.05 :25.91% 43 98 5000

1 50 1 67 Tmmur " " i" " I" ■' i" ‘' i" " I THTT ICIUI00"01—T090111717T r •1 ‘ p'1 • i _1’111101111011111’1117 TTrp miz- 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 4.90 5.00 5.10 5.20 5.30 5.40

26680.D NP112701.M Fri Dec 07 13:11:26 2001 Page 1

NYC-WTC_000032065

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