GCMS analysis results for sample AD26680, Dec 10 2001

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Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0401\26680.D Vial: 3 Acq On 4 Dec 2001 12:38 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Oxepane, 2,2,4-trimethyl- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

5.10 1.46 ng/uL 391502 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Oxepane, 2,2,4 trimethyl - 100 C6H120 023120-44-7 36 2 1-Hexene 84 C6H12 000592-41-6 33 3 Pentanal, 3-methyl- 100 C6H120 015877-57-3 23 4 Pentane, 2 ,3-dimethyl- 100 C7H16 000565-59-3 17 Abundance < Scan 28 (5.102 min): 26680.D (-) m/z 41 05 100.00% 41 56

5000-

45 71 i >' ■' i'' ■' r ■'' i T''' 1 I 4.90 5.00 5.10 5.20 5.30 5.40 5.50

m/z—> 111'' I 5t4 4 1——uktu 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 67 —I —Tup PTTTTTT) 100 m/z 56,10 77.41% Abundance #1525: Oxepane. 2,2,4-trimethyl- 43 59

5000 TTTT TIIm—uprr 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m/ z 59 10 71.17% 31 55 I 85

m/z-> 20 25 30 35 40 45 50 55 60 H i" " i TTT TTTT 65 70 75 80 85 90 IWTBIPgum 100 95 100 105 Abundance #62755: 1-Hexene 41 56 27 I’’ "II’II’I’T’IT 4.90 5.00 5.10 5.20 5.30 5.40 5.50 5000- m/ z 42.05 62.86% 84 69 51 . I' *'' I i'1' ■ i' ■1 ■ i I ■1' ’ i I' " • I I | I « I I | l t I'. | I > . t | . I ! < | . . < . | I . i I | . I I . | I I < . )

m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63404: Pentanal, 3-methyl- T’TTTTTTTTETITTTTT’Ir 56 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m/z 43 05 59.29% / 5000

27 44 71

m/z—> l - 7.4 20 25 30 35 40 45 50 55 60 65 70 82 11" " 11" 75 80 85 90 100 95 100 105 1 T‘I——0——1111TETEIITTTTTTTTT | 4.90 5.00 5.10 5.20 5.30 5.40 5.50

26680.D NP112701.M Fri Dec 07 13:11:28 2001 Page 2

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