GCMS analysis results for sample AD26625, Dec 10 2001

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Library Search Compound Report

• Data File C:\HPCHEM\l\DATA\DEC0601\26625.D Vial: 8 Acq On 6 Dec 2001 4:34 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Oxepane, 2,2,4-trimethyl- Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

5.12 1.46 ng/uL 471635 1,4-Dichlorobenzene-d4 11.88

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Oxepane, 2,2,4 - trimethyl - 100 C6H120 023120-44-7 25 2 1-Pentanol, 4-me yl- 102 C6H140 000626-89-1 25 3 1-Hexene / 84 C6H12 000592-41-6 25 4 1-Hexene 84 C6H12 _______ 000592-41-6 25 Abundance Scan 31 (5.124 min): 26625.D (-) m/z 41.10 100.00% 41 56

5000

45 71 1’1’13 TUTTIT 50 67 | 4.90 5.00 5.10 5.20 5.30 5.40 5.50

m/z-> " 111111''" i 37 TT+ 5t+ +frrTI..... T’I"t"ITTTTTTTTTTT 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 100 TTMIT m/z 56 *4 10 80.64% Abundance #1525: Oxepane, 2,2,4-trimethyl- I 43 59

5000 I ’ ‘ “ I 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m/z 59.10 76.42% | m/z-> 20 25 30 31 35 40 +l. 45 50 55 60 65 70 75 80 ' ।1 ■ ■' ।1 TTTTTT " । ■ 85 “I ’il TUUU 100 85 90 95 100 105 Abundance #53578: 1-Pentanol. 4-methyl- 56 41 TT 69 4.90 5.00 5.10 5.20 5.30 5.40 5.50 5000 m/z 42.05 63.84%

m/z-> Abundance 20 ' I" " 1111' I ‘ 25 30 45 : 60 T1I TUUnT i r > r r»j 35 40 45 50 55 60 65 70

41 #62753: 1-Hexene 56 84 T" 11111 ’' I 75 80 85 T’ITTTTTTT’"’’’’’’ 90 95 100 105 J TTTTTTIUTTTTDTT 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m/z ,43.05 62.48% 5000 27 84 69

■ ‘ i'' ■ ■ i' T ..... '"I —52. ■ • i " • ■ i ■ ■ i " '' i1TTTTTT T’’’’I"""110ETIIETTTI’TTI m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 4.90 5.00 5.10 5.20 5.30 5.40 5.50

26625.D NP112701.M Fri Dec 07 14:48:33 2001 Page 2

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