GCMS comments for sample AD26475 showing no non-target compounds

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C : \HPCHEM\ 1 \DATA\DECO7 01\26475.D Vial: 5 Acq On 7 Dec 2001 9:45 pm Operator: GALOS Sample gc/ms unknown 11/6 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Oxirane, 2-methyl-3-propyl-, c Concentration Rank 12

R..T. EstConc Area Relative to ISTD R.T.

5.64 0.47 ng/uL 133131 1,4-Dichlorobenzene-d4' 11.88

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Oxirane, 2-methyl-3-propyl-, cis- 100 C6H120 006124-90-9 36 2 Heptane, 2,3 -dimethyl - 128 C9H20 003074-71-3 17 3 1-Cyclob tylethanol 100 C6H120 038401-41-1 17 4 Oxirane/ 2-methyl-3-propyl-, trans- 100 C6H120 006124-91-0 17 Abundance Scan 87 (5.637 min): 26475.D (-) m/z 41.05 100.00% 41

57 85 5000

51 71 ......A 5.20 5.40 5.60 5.80 6.00 ....— - — _ ....... | . ' i ■ ' ' ■ i m/z 45.10 97.10% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #1531: Oxirane, 2-methyl-3-propyl-, cis- 43 __

57 5000 71 85 —I I PMATYI 4 4 PrA 5.20 5.40 5.60 5.80 . 6.00 m/z 43.10 80.75%

m/z-> 20 ... 4 30 40 —— 50 60 70 80 90 100 100 110 120 130 Abundance #65133: Heptane, 2.3-dimethyl- 43

5.20 5.40 5.60 5.80 6.00 5000- m/z 57.00 57.05% 84 27 57 71 I I. III , 1......................... 128 m/z-> Abundance ' Tmu | 1 1 1 1 I ri ' ■ i ■ • ■ ■ । ■ 20 30 40

43 50

57 60 70 80 #1544: 1-Cyclobutylethanol 90 100 110 120 130

5.20 A 5.40 5.60 5.80 6.00

N 71 m/ z 85.05 !54.66% 5000 - 27

85 ■ 1111—1-| । > 1111 — h 1 1 11 i 1 -........—............. m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 5.20 5.40 5.60 5.80 6.00

26475.D NP112701.M Thu Dec 13 11:19:30 2001 Page 4

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